顺式-2-(6-氨基-9H-嘌呤-9-基)-环己醇合成路线 （共 3 条）
反应条件
1: Ph3P, diisopropyl azodicarboxylate / tetrahydrofuran / 48 h / Ambient temperature
2: Et3N / H2O; methanol / 4 h / 80 °C
3: H2 / Pd/C / acetic acid; aq. HCl / 16 h / Ambient temperature
View Scheme
参考文献
Liboska, Radek; Masojidkova, Milena; Rosenberg, Ivan
Collection of Czechoslovak Chemical Communications, 1996 , vol. 61, # 5 p. 778 - 790
反应条件
1: 98 percent / dimethylformamide / 2 h / Ambient temperature
2: Ph3P, diisopropyl azodicarboxylate / tetrahydrofuran / 48 h / Ambient temperature
3: Et3N / H2O; methanol / 4 h / 80 °C
4: H2 / Pd/C / acetic acid; aq. HCl / 16 h / Ambient temperature
View Scheme
参考文献
Liboska, Radek; Masojidkova, Milena; Rosenberg, Ivan
Collection of Czechoslovak Chemical Communications, 1996 , vol. 61, # 5 p. 778 - 790
反应条件
1: Ph3P, diisopropyl azodicarboxylate / tetrahydrofuran / 48 h / Ambient temperature
2: Et3N / H2O; methanol / 4 h / 80 °C
3: H2 / Pd/C / acetic acid; aq. HCl / 16 h / Ambient temperature
View Scheme
参考文献
Liboska, Radek; Masojidkova, Milena; Rosenberg, Ivan
Collection of Czechoslovak Chemical Communications, 1996 , vol. 61, # 5 p. 778 - 790
