3-苯基异噁唑-5-甲醛合成路线 （共 11 条）
反应条件
1: With oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-78°C; 0.5 h; 2: With triethylamine in dichloromethane T=-78 - 20°C;
参考文献
Du, Chao; Li, Liqi; Li, Ying; Xie, Zhixiang
Angewandte Chemie - International Edition, 2009 , vol. 48, # 42 p. 7853 - 7856
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Synlett, , # 6 p. 919 - 923
反应条件
1.1: N-chloro-succinimide / dichloromethane / 0.67 h / 20 °C 1.2: 4 h / Reflux 2.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 6 p. 831 - 842
反应条件
sodium ethanolate T=140 - 160°C; Erhitzen des Reaktionsprodukts mit wss. HCl;
参考文献
Gazzetta Chimica Italiana, , vol. 73, p. 99,103
反应条件
1.1: hydroxylamine hydrochloride / methanol; water / 20 °C 1.2: 4 h 2.1: N-chloro-succinimide / dichloromethane / 0.67 h / 20 °C 2.2: 4 h / Reflux 3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 6 p. 831 - 842
参考文献
Atti della Societa Peloritana di Scienze Fisiche, Matematiche e Naturali, , vol. 5, p. 159,166
参考文献
Gazzetta Chimica Italiana, , vol. 73, p. 99,103
反应条件
palladium diacetate; potassium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in acetone T=50°C; Inert atmosphereGlovebox;
参考文献
Tschaen, Brittany A.; Schmink, Jason R.; Molander, Gary A.
Organic Letters, 2013 , vol. 15, # 3 p. 500 - 503
反应条件
potassium dichromate; sulfuric acid
参考文献
Panizzi
Gazzetta Chimica Italiana, 1943 , vol. 73, p. 99,103
参考文献
Panizzi
Gazzetta Chimica Italiana, 1943 , vol. 73, p. 99,103
