1-(丁氧基-甲氧基-磷酰)氧基丁烷合成路线 (共 8 条)
参考文献
Morales,J.G. et al.
Journal of Medicinal Chemistry, 1972 , vol. 15, p. 1225 - 1231
反应条件
methanesulfonic acid; dimethylsulfide 18 h; Ambient temperature;
参考文献
Synthesis, , # 6 p. 451 - 452
反应条件
sodium hydroxide; tetrabutylammomium bromide in tetrachloromethane; dichloromethane
T=15°C; 3 h;
参考文献
Ilia, Gheorghe; Popa, Adriana; Iliescu, Smaranda; Bora, Alina; Dehelean, Gheorghe; Pascariu, Aurelia
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 7 p. 1513 - 1519
反应条件
in various solvent(s)
T=80°C; 1 h;
参考文献
Yoshino, Tomonori; Imori, Satomi; Togo, Hideo
Tetrahedron, 2006 , vol. 62, # 6 p. 1309 - 1317
反应条件
cesium fluoride in acetonitrile
6 h; Ambient temperature;
参考文献
Takaku, Hiroshi; Kamaike, Kazuo; Mori, Hisashi; Ishido, Yoshiharu
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 2157 - 2159
反应条件
oxygen; methylene blue in acetonitrile
T=20°C; 0.166667 h; Irradiationwithout methanol; other reaction time; also in the presence of diphenyl sulfides or sulfoxides as trapping agents of intermediates; MechanismProduct distribution;
参考文献
Tsuji, Shoei; Kondo, Masaaki; Ishiguro, Katsuya; Sawaki, Yasuhiko
Journal of Organic Chemistry, 1993 , vol. 58, # 19 p. 5055 - 5059
参考文献
Burger; Wagner
Journal of Chemical and Engineering Data, 1958 , vol. 3, p. 310
反应条件
T=60°C; Rate constant;
参考文献
Lebedev, N. N.; Mamzurin, B. V.; Savel'yanov, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 3 p. 546 - 549,482 - 485