1,2-双(羧甲硫基)-乙烷合成路线 （共 10 条）
反应条件
hydrogenchloride; sodium hydroxide in ethanol; water
参考文献
Schering Corporation
Patent: US4156683 A1, 1979 ;
反应条件
sodium hydroxide
anschliessend mit Chloressigsaeure;
参考文献
Schenley Ind.
Patent: US2657231 , 1950 ;
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Farbenfabr.Bayer
Patent: DE831246 , 1951 ;
DRP/DRBP Org.Chem.
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride
1.) aq. EtOH, reflux, 3 h, 2.) aq. EtOH, 60 deg C; Yield given. Multistep reaction;
参考文献
Jian-Hua, Wang; Zhen, Zhang; Yong-Lai, Feng
Synthetic Communications, 1993 , vol. 23, # 3 p. 373 - 377
参考文献
BASF
Patent: DE840997 , 1951 ;
DRP/DRBP Org.Chem.
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Goodrich Co.
Patent: US2602816 , 1947 ;
反应条件
ethanol; potassium carbonate
参考文献
Chivers; Smiles
Journal of the Chemical Society, 1928 , p. 701
参考文献
Voronkov, M. G.; Zhila, G. Yu.; Vlasova, N. N.; Yarosh, O. G.; Albanov, A. I.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 8 p. 1827 - 1831,1631 - 1633
参考文献
Voronkov, M. G.; Zhila, G. Yu.; Vlasova, N. N.; Yarosh, O. G.; Albanov, A. I.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 8 p. 1827 - 1831,1631 - 1633
反应条件
Kochen des Reaktionsprodukts mit konz.Salzsaeure;
参考文献
Chivers; Smiles
Journal of the Chemical Society, 1928 , p. 701
反应条件
dihydrogen peroxide in acetic anhydride; acetic acid
T=0 - 5°C; 4 h;
参考文献
Baliah, V.; Aparajithan, K.; Prema, S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 8 p. 716 - 718
反应条件
das Kaliumsalz reagiert;
参考文献
Tiberg
Chemische Berichte, 1916 , vol. 49, p. 2027
