1-硝基-4-丙氧基-苯合成路线 (共 18 条)
反应条件
hydrazine hydrate; carbon in ethanol 2 h; Heating;
参考文献
Han, Byung Hee; Shin, Dae Hyun; Cho, Sung Yun
Tetrahedron Letters, 1985 , vol. 26, # 50 p. 6233 - 6234
反应条件
hydrogenchloride; zinc
参考文献
Chaudhuri, Narayan C.
Synthetic Communications, 1996 , vol. 26, # 20 p. 3783 - 3790
反应条件
1: (reduction) 2: ethanol; acetic acid View Scheme
参考文献
Murase,K.; Watanabe,H.
Bulletin of the Chemical Society of Japan, 1973 , vol. 46, p. 3142 - 3143
反应条件
hydrogen; palladium nanoparticles in toluene
T=20°C; 4 h;
参考文献
Pieber, Bartholomaeus; Martinez, Sabrina Teixeira; Cantillo, David; Kappe, C. Oliver
Angewandte Chemie - International Edition, 2013 , vol. 52, # 39 p. 10241 - 10244
Angew. Chem., 2013 , p. 10431 - 10434
反应条件
1: 4-fluoro-nitro-benzene With cesium fluoride in N,N-dimethyl-formamide
0.166667 h; Inert atmosphere;
2: trimethyl(propoxy)silane in N,N-dimethyl-formamide
T=95°C; 40 h;
参考文献
Zylum Beteiligungsgesellschaft mbH and Co. Patente II KG
Patent: US2012/142937 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
potassium carbonate in acetone
72 h; Ambient temperature;
参考文献
Matthews, Susan E.; Saadioui, Mohamed; Boehmer, Volker; Barboso, Silvia; Arnaud-Neu, Francoise; Schwing-Weill, Marie-Jose; Carrera, Alejandro Garcia; Dozol, Jean-Francois
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 1999 , vol. 341, # 3 p. 264 - 273
反应条件
potassium carbonate in acetonitrile
8 h; Reflux;
参考文献
Ho, I-Ting; Chu, Jean-Ho; Chung, Wen-Sheng
European Journal of Organic Chemistry, 2011 , # 8 p. 1472 - 1481
反应条件
1: propan-1-ol With N-benzyl-trimethylammonium hydroxide
0.166667 h; Neat (no solvent);
2: 4-fluoro-nitro-benzene T=50°C; 0.5 h; Neat (no solvent);
参考文献
Meshram; Goud, P. Ramesh; Reddy, B. Chennakesava; Kumar, D. Aravind
Synthetic Communications, 2010 , vol. 40, # 14 p. 2122 - 2129
反应条件
hydrogen; palladium nanoparticles in toluene
T=20°C; 24 h;
参考文献
Callis, Nuria Miro; Thiery, Emilie; Le Bras, Jean; Muzart, Jacques
Tetrahedron Letters, 2007 , vol. 48, # 46 p. 8128 - 8131
反应条件
water; copper (II) acetate monohydrate; caesium carbonate; triphenyl-phosphine oxide
T=145°C; Inert atmosphere;
参考文献
Wang, Feng; Tang, Boxiao; Xie, Yexiang; Li, Jinheng
Chinese Journal of Chemistry, 2010 , vol. 28, # 11 p. 2318 - 2322