2-羟基-2-甲基-3-氧丁酸甲酯合成路线 (共 4 条)
反应条件
oxygen; cerium(III) chloride in isopropyl alcohol
T=23°C; P=760 Torr; 16 h;
参考文献
Christoffers, Jens; Kauf, Thomas; Werner, Thomas; Roessle, Michael
European Journal of Organic Chemistry, 2006 , # 11 p. 2601 - 2608
反应条件
potassium permanganate; acetic acid in water; acetone
T=-10°C; 1 h;
参考文献
Crout, D. H. G.; Rathbone, D. L.
Synthesis, 1989 , # 1 p. 40 - 42
反应条件
di(n-butyl)tin oxide in toluene
22 h; Heating;
参考文献
Crout, David H. G.; Rathbone, Daniel L.
Journal of the Chemical Society, Chemical Communications, 1987 , # 4 p. 290 - 291
反应条件
1: 50 percent / DBU / diethyl ether / 16 h / 23 °C
2: 52 percent / O2 / CeCl3*7H2O / propan-2-ol / 16 h / 23 °C / 760 Torr
View Scheme
参考文献
Christoffers, Jens; Kauf, Thomas; Werner, Thomas; Roessle, Michael
European Journal of Organic Chemistry, 2006 , # 11 p. 2601 - 2608