2,3-二(4-甲氧基苯基)喹喔啉合成路线 （共 12 条）
参考文献
Aghapoor, Kioumars; Darabi, Hossein Reza; Mohsenzadeh, Farshid; Balavar, Yadollah; Daneshyar, Hesam
Transition Metal Chemistry, 2010 , vol. 35, # 1 p. 49 - 53
反应条件
morpholine; anhydrous iron chloride in ethanol
T=80°C; 1.5 h;
参考文献
Liu, Peng; Lei, Min; You, Hanyun; Chen, Xubing; Chen, Hu; Ma, Lei; Hu, Lihong
Synthetic Communications, 2012 , vol. 42, # 2 p. 236 - 245
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; toluene
Suzuki-Miyaura coupling; 48 h; Heating;
参考文献
Mao, Lisheng; Sakurai, Hidehiro; Hirao, Toshikazu
Synthesis, 2004 , # 15 p. 2535 - 2539
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide
T=90°C; 12 h;
参考文献
Qi, Chaorong; Jiang, Huanfeng; Huang, Liangbin; Chen, Zhengwang; Chen, Huoji
Synthesis, 2011 , # 3 art. no. F17110SS, p. 387 - 396
反应条件
ammonium cerium(IV) nitrate; air in water
T=20°C; 0.833333 h;
参考文献
Shaabani, Ahmad; Maleki, Ali
Chemical and Pharmaceutical Bulletin, 2008 , vol. 56, # 1 p. 79 - 81
反应条件
tin(ll) chloride in ethanol; water
1 h; Reflux;
参考文献
Shi, Da-Qing; Dou, Guo-Lan; Ni, Sai-Nan; Shi, Jing-Wen; Li, Xiao-Yue
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 6 p. 1797 - 1801
反应条件
1: 1,3-dimethyl-1H-benzo[d]imidazol-3-ium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 5 h / 0 °C / |Inert atmosphere
2: 1,8-diazabicyclo[5.4.0]undec-7-ene; oxygen / N,N-dimethyl-formamide; ethyl acetate / 6 h / 70 °C
3: N,N-dimethyl-formamide; ethyl acetate / 1.5 h / 20 °C
View Scheme
参考文献
Lin, Yang; Lei, Xiaoli; Yang, Qin; Yuan, Jiangjun; Ding, Qiuping; Xu, Jingshi; Peng, Yiyuan
Synthesis (Germany), 2012 , vol. 44, # 17 p. 2699 - 2706
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; oxygen / N,N-dimethyl-formamide; ethyl acetate / 6 h / 70 °C
2: N,N-dimethyl-formamide; ethyl acetate / 1.5 h / 20 °C
View Scheme
参考文献
Lin, Yang; Lei, Xiaoli; Yang, Qin; Yuan, Jiangjun; Ding, Qiuping; Xu, Jingshi; Peng, Yiyuan
Synthesis (Germany), 2012 , vol. 44, # 17 p. 2699 - 2706
反应条件
1: Grubb's 2nd generation catalyst; tetra-(n-butyl)ammonium iodide; tert.-butylhydroperoxide / toluene; acetonitrile; water / 1 h / 20 °C / |Inert atmosphere
2: acetic acid / toluene; acetonitrile; water / 2 h / 60 °C / |Inert atmosphere
View Scheme
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
反应条件
1: Grubb's 2nd generation catalyst / toluene / 1.5 h / 80 °C / |Inert atmosphere
2: Grubb's 2nd generation catalyst; tetra-(n-butyl)ammonium iodide; tert.-butylhydroperoxide / toluene; acetonitrile; water / 1 h / 20 °C / |Inert atmosphere
3: acetic acid / toluene; acetonitrile; water / 2 h / 60 °C / |Inert atmosphere
View Scheme
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
