4’-甲氧基联苯-3-羧酸合成路线 （共 14 条）
反应条件
1: With potassium hydroxide in ethanol; water T=120°C; 0.5 h; Microwave irradiation; 2: With hydrogenchloride in water
参考文献
Bang, Joon Seok; Kim, Young Jin; Song, Jiho; Yoo, Jong-Sun; Lee, Seul; Lee, Mi Ji; Min, Hyeyoung; Hwang, Kwang Woo; Min, Kyung Hoon
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 17 p. 5262 - 5268
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: 3-bromophenylacetic acid in tetrahydrofuran T=0 - 25°C; 18 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
反应条件
potassium carbonate; dichlorobis(4-pyridinaldoxime)palladium(II) in water Suzuki reaction; 1 h; Heating;
参考文献
Evdokimov; Bumagin
Russian Chemical Bulletin, 2007 , vol. 56, # 2 p. 369 - 370
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol T=100°C; Suzuki-Miyaura reaction; 6 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
sodium hydroxide in methanol; water 2 h; Reflux;
参考文献
Dai, Jun; Zhou, Kaifeng; Li, Ming; Sun, Huiqin; Chen, Yunqing; Su, Shijian; Pu, Xuemei; Huang, Yan; Lu, Zhiyun
Dalton Transactions, 2013 , vol. 42, # 29 p. 10559 - 10571
反应条件
potassium permanganate
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
1: diethyl ether / Erhitzen des Reaktionsprodukts mit Essigsaeure, Acetanhydrid und Naphthalin-2-sulfonsaeure und anschliessend mit Schwefel 2: KMnO4 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
1: diethyl ether / Erhitzen des Reaktionsprodukts mit Essigsaeure, Acetanhydrid und Naphthalin-2-sulfonsaeure und anschliessend mit Schwefel 2: KMnO4 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 75, p. 4969,4972
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 2 h / |Reflux 2: potassium hydroxide / water; ethanol / 0.5 h / 120 °C / |Microwave irradiation View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 17 p. 5262 - 5268
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / tetrahydrofuran; water / 2 h / |Reflux 2: potassium hydroxide / water; ethanol / 0.5 h / 120 °C / |Microwave irradiation View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 17 p. 5262 - 5268
