3-(3-甲氧基苯基)-1-丙醇合成路线 （共 22 条）
反应条件
5 palladium on charcoal; hydrogen in methanol
12 h; Inert atmosphere;
参考文献
Zhao, Peng; Beaudry, Christopher M.
Organic Letters, 2013 , vol. 15, # 2 p. 402 - 405
反应条件
1: 94.8 percent / pyridine, piperidine
2: 96.3 percent / H2 / 10percent Pd/C / methanol
3: 87.2 percent / LiAlH4 / diethyl ether
View Scheme
参考文献
Venit, John J.; DiPierro, Michael; Magnus, Philip
Journal of Organic Chemistry, 1989 , vol. 54, # 18 p. 4298 - 4301
反应条件
1: With 9-borabicyclo[3.3.1]nonane dimer
2: With sodium hydroxide; dihydrogen peroxide
参考文献
Burlingame, Mark A.; Shaw, Simon J.; Sundermann, Kurt F.; Zhang, Dan; Petryka, Joseph; Mendoza, Esteban; Liu, Fenghua; Myles, David C.; LaMarche, Matthew J.; Hirose, Tomoyasu; Freeze, B. Scott; Smith III, Amos B.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 9 p. 2335 - 2338
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Kita, Yasuyuki; Egi, Masahiro; Ohtsubo, Makoto; Saiki, Toyokazu; Okajima, Akiko; Takada, Takeshi; Tohma, Hirofumi
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 2 p. 241 - 245
反应条件
lithium aluminium tetrahydride
参考文献
Pearson, Anthony J.; Ghidu, Victor P.
Journal of Organic Chemistry, 2004 , vol. 69, # 25 p. 8975 - 8978
反应条件
1.1: 9-BBN
1.2: aq. H2O2; NaOH
View Scheme
参考文献
Burlingame, Mark A.; Shaw, Simon J.; Sundermann, Kurt F.; Zhang, Dan; Petryka, Joseph; Mendoza, Esteban; Liu, Fenghua; Myles, David C.; LaMarche, Matthew J.; Hirose, Tomoyasu; Freeze, B. Scott; Smith III, Amos B.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 9 p. 2335 - 2338
反应条件
magnesium; ethylene dibromide
1.) ether, reflux, 1 h; 2.) ether, RT, 24 h; Yield given. Multistep reaction;
参考文献
Parlow, John J.
Tetrahedron, 1994 , vol. 50, # 11 p. 3297 - 3314
反应条件
(i), (ii) (esterification), (iii) LiAlH4; Multistep reaction;
参考文献
Ando,T. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 219 - 224
反应条件
1: PCC
2: 75 percent / <OH(CH2)2C3HNC(CH3)Bn>Cl, Et3N / ethanol
View Scheme
参考文献
Tedesco, Rosanna; Katzenellenbogen, John A.; Napolitano, Elio
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 22 p. 2919 - 2924
反应条件
carbon tetrabromide; triphenylphosphine in diethyl ether
reflux, 1 h, 2 h, 15 h;
参考文献
Maskill, H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1739 - 1742
