n-butyllithium; magnesium bromide in tetrahydrofuran; diethyl ether; hexane T=-78°C; warming to room temperature; Yield given. Title compound not separated from byproducts;
参考文献
Dhawan, Kasturi L.; Gowland, Barbara D.; Durst, Tony
Journal of Organic Chemistry, 1980 , vol. 45, # 5 p. 922 - 924