1-(4-甲氧基苯基)吡啶-2(1H)-酮合成路线 (共 5 条)
反应条件
copper(l) iodide; tetrabutyl-ammonium chloride; sodium hydride in N,N-dimethyl-formamide
T=110°C; 12 h; Product distribution / selectivity;
参考文献
Zhang, Huiping; Chen, Bang-Chi; Zhao, Rulin
Patent: US2006/69260 A1, 2006 ;
Location in patent: Page/Page column 11 ;
反应条件
potassium phosphate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane
T=110°C; 22 h;
参考文献
Li, Chun Sing; Dixon, Darryl D.
Tetrahedron Letters, 2004 , vol. 45, # 22 p. 4257 - 4260
反应条件
copper(l) iodide in N,N-dimethyl-formamide
T=110°C; 12 h; Product distribution / selectivity;
参考文献
Zhang, Huiping; Chen, Bang-Chi; Zhao, Rulin
Patent: US2006/69260 A1, 2006 ;
Location in patent: Page/Page column 10-11 ;
反应条件
potassium carbonate; copper(l) iodide in N,N-dimethyl-formamide
T=150°C; 21 h;
参考文献
BANYU PHARMACEUTICAL CO., LTD.
Patent: WO2006/59778 A1, 2006 ;
Location in patent: Page/Page column 43 ;
WO 2006/059778 A1
反应条件
potassium tert-butylate in tetrahydrofuran
3 h; Heating;
参考文献
Ikegai, Kazuhiro; Nagata, Yuzo; Mukaiyama, Teruaki
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 5 p. 761 - 767