3-氯-9H-芴-9-酮合成路线 （共 20 条）
反应条件
ethanol
Diazotization;
参考文献
Bell; Gibson
Journal of the Chemical Society, 1955 , p. 3560
反应条件
1: PCl5; chlorobenzene; AlCl3 / weiteres Reagens: H2SO4
2: aqueous H2SO4 / Diazotization
View Scheme
参考文献
Bell; Gibson
Journal of the Chemical Society, 1955 , p. 3560
反应条件
1: CHCl3; chlorine
2: Na2Cr2O7
4: ethanol / Diazotization
View Scheme
参考文献
Bell; Gibson
Journal of the Chemical Society, 1955 , p. 3560
反应条件
1: Na2Cr2O7
3: ethanol / Diazotization
View Scheme
参考文献
Bell; Gibson
Journal of the Chemical Society, 1955 , p. 3560
反应条件
2: ethanol / Diazotization
View Scheme
参考文献
Bell; Gibson
Journal of the Chemical Society, 1955 , p. 3560
反应条件
1: dipotassium peroxodisulfate; palladium diacetate; trifluoroacetic acid / 15 h / 120 °C / Inert atmosphere
2: hydrogenchloride; water / 100 °C / Inert atmosphere
View Scheme
参考文献
Thirunavukkarasu, Vedhagiri S.; Cheng, Chien-Hong
Chemistry - A European Journal, 2011 , vol. 17, # 52 p. 14723 - 14726
反应条件
(i) (diazotization), (ii) CuCl; Multistep reaction;
参考文献
Smith,G.G.; Bayer,R.P.
Tetrahedron, 1962 , vol. 18, p. 323 - 331
反应条件
1: 40 percent
2: 75 percent
View Scheme
参考文献
Bolton, Roger; Mguni, Raphael S.; Williams, Gareth H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 405 - 408
反应条件
1: 40 percent
2: 75 percent
View Scheme
参考文献
Bolton, Roger; Mguni, Raphael S.; Williams, Gareth H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1986 , p. 405 - 408
反应条件
sodium tetrahydroborate in isopropyl alcohol
T=25 - 45°C; Kinetics;
参考文献
Smith,G.G.; Bayer,R.P.
Tetrahedron, 1962 , vol. 18, p. 323 - 331
