4-硝基苯甲酸苯甲酰甲基酯合成路线 (共 9 条)
反应条件
N-bromosuccinmide; oxygen; 5-(2-hydroxyethyl)-4-methyl-3-(phenylmethyl)thiazolium chloride; triethylamine in dimethyl sulfoxide
T=25°C; P=760.051 Torr; 18 h; Reagent/catalystSolvent; regioselective reaction;
参考文献
Reddi, Rambabu N.; Malekar, Pushpa V.; Sudalai, Arumugam
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 38 p. 6477 - 6482
反应条件
PEG-400; sodium hydrogencarbonate; sodium iodide in acetonitrile
T=80°C; 5 h;
参考文献
Hu; Pa; Cui; Wang
Synthetic Communications, 1992 , vol. 22, # 19 p. 2763 - 2767
反应条件
potassium fluoride in N,N-dimethyl-formamide
1 h; Ambient temperature;
参考文献
Miller, Jack M.; Brindle, Ian D.; Cater, Stephen R.; So, Kwok-Hung; Clark, James H.
Analytical Chemistry, 1980 , vol. 52, # 14 p. 2430 - 2432
反应条件
dibenzo-18-crown-6; tetrabutylammomium bromide in acetonitrile
3 h; Ambient temperature;
参考文献
Jugdale; Patil; Salunkhe
Synthetic Communications, 1996 , vol. 26, # 9 p. 1747 - 1752
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate
T=20°C; 0.333333 h;
参考文献
Liu, Zhi; Chen, Zhen-Chu; Zheng, Qin-Guo
Synthesis, 2004 , # 1 p. 33 - 36
反应条件
sodium carbonate
T=20°C; 0.5 h; Ionic liquid;
参考文献
Le, Zhang-Gao; Xie, Zong-Bo; Xu, Jian-Ping
Synthetic Communications, 2009 , vol. 39, # 4 p. 743 - 747
反应条件
triethylamine in acetonitrile
Heating;
参考文献
Prakash, Om; Saini, Neena; Sharma, Pawan Kumar
Journal of the Indian Chemical Society, 1995 , vol. 72, # 2 p. 129 - 132
参考文献
Rather; Reid
Journal of the American Chemical Society, 1919 , vol. 41, p. 79
反应条件
1: acetonitrile / 2 h / Heating
2: 62 percent / Et3N / acetonitrile / Heating
View Scheme
参考文献
Prakash, Om; Saini, Neena; Sharma, Pawan Kumar
Journal of the Indian Chemical Society, 1995 , vol. 72, # 2 p. 129 - 132