1: 82 percent / K2CO3, NaI / dimethylformamide / 1.5 h / 100 °C / var.: THF, LDA, -70 deg C 2: 80 percent / DCC, DMSO, pyridine, TFA / benzene / 1) 0 deg C 2) RT, 24 h View Scheme
参考文献
Reese, Colin B.; Thompson, Elizabeth A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2881 - 2886
1: K2CO3; NaI / dimethylformamide / 100 °C 2: DCC; DMSO; TFA / benzene; pyridine View Scheme
参考文献
Lloyd, Wayne; Reese, Colin B.; Song, Quanlai; Vandersteen, Anthony M.; Visintin, Cristina; Zhang, Pei-Zhou
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 165 - 176
1: K2CO3; NaI / dimethylformamide / 100 °C 2: DCC; DMSO; TFA / benzene; pyridine View Scheme
参考文献
Reese, Colin B.; Thompson, Elizabeth A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2881 - 2886
potassium carbonate; sodium iodide in N,N-dimethyl-formamide T=100°C; Alkylation; Cyclization;
参考文献
Lloyd, Wayne; Reese, Colin B.; Song, Quanlai; Vandersteen, Anthony M.; Visintin, Cristina; Zhang, Pei-Zhou
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 165 - 176
1: K2CO3; NaI / dimethylformamide / 100 °C
2: DCC; DMSO; TFA / benzene; pyridine
View Scheme
参考文献
Lloyd, Wayne; Reese, Colin B.; Song, Quanlai; Vandersteen, Anthony M.; Visintin, Cristina; Zhang, Pei-Zhou
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 165 - 176
potassium carbonate; sodium iodide in N,N-dimethyl-formamide
T=100°C; Alkylation; Cyclization;
参考文献
Lloyd, Wayne; Reese, Colin B.; Song, Quanlai; Vandersteen, Anthony M.; Visintin, Cristina; Zhang, Pei-Zhou
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 165 - 176
1: K2CO3; NaI / dimethylformamide / 100 °C
2: DCC; DMSO; TFA / benzene; pyridine
View Scheme
参考文献
Lloyd, Wayne; Reese, Colin B.; Song, Quanlai; Vandersteen, Anthony M.; Visintin, Cristina; Zhang, Pei-Zhou
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 165 - 176
