反应条件
1.1: BH3*THF / tetrahydrofuran / 20 h / 20 °C
1.2: 850 mg / polymer-supported triethylamine carbonate; aq. H2O2; polymer-supported trimethylamine thiosulfate / tetrahydrofuran; methanol
2.1: 98 percent / morpholinomethyl polystyrene / CH2Cl2 / 20 h / 20 °C
3.1: 77 percent / DIBAL-H / hexane; tetrahydrofuran / 1 h / -78 °C
4.1: 100 percent / pyridinium chloroformate/basic alumina / CH2Cl2 / 20 h / 20 °C
5.1: 98 percent / diethyl ether; tetrahydrofuran / 2 h / -78 °C
6.1: 98 percent / pyridinium chlorochromate/basic alumina / CH2Cl2 / 20 h / 20 °C
View Scheme
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Brown, Dearg S.; Baxendale, Ian R.; Ley, Steven V.
Chemistry - A European Journal, 2004 , vol. 10, # 10 p. 2529 - 2547
