4-氯-4-(甲基硫代)苯甲酮合成路线 (共 2 条)
反应条件
AlCl3, aluminium chloride in 1,2-dichloro-ethane
T=-5 - 5°C;
参考文献
Insight High Technology Co., Ltd.; ZHAO, Wenchao; MA, Zhongli; LI, Jiaqi; YAO, Lixiu; ZHANG, Jue; HU, Weijing; LI, Jing; WANG, Yonglin
Patent: EP2738159 A1, 2014 ;
Location in patent: Paragraph 0047 ;
反应条件
molybdenum dichloride dioxide
Friedel Crafts acylation; 20 h; Inert atmosphereNeat (no solvent)Reflux;
参考文献
de Noronha, Rita G.; Fernandes, Ana C.; Romao, Carlos C.
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1407 - 1410