(1R)-10-樟脑磺酰胺合成路线 （共 6 条）
反应条件
pyridine; Rink amide resin; trifluoroacetic acid 1.) CH2Cl2, room temp., 15 h, 2.) CH2Cl2, 15 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 37, # 8 p. 1145 - 1148
参考文献
Helvetica Chimica Acta, , vol. 67, p. 1397 - 1401
反应条件
1: 99.3 percent / NaOMe / methanol / 64 h / Ambient temperature 2: 1.) LiAlH4; 2.) 1N aq. HCl / 1.) THF, 0 deg C, 2.) r.t., 1 h 3: 88 percent / NaH / toluene / 3 h / Ambient temperature View Scheme
参考文献
Vandewalle, M.; Van der Eycken, J.; Oppolzer, W.; Vullioud, C.
Tetrahedron, 1986 , vol. 42, # 14 p. 4035 - 4044
反应条件
sodium methylate in methanol 64 h; Ambient temperature;
参考文献
Vandewalle, M.; Van der Eycken, J.; Oppolzer, W.; Vullioud, C.
Tetrahedron, 1986 , vol. 42, # 14 p. 4035 - 4044
反应条件
1: 95 percent / Amberlyst 15 ion-exchange resin / tetrahydrofuran / 4 h / Heating 2: Oxone, K2CO3 / tetrahydrofuran; H2O / Ambient temperature View Scheme
参考文献
Davis,F.A.; Towson,J.C.; Weismiller,M.C.
Journal of the American Chemical Society, 1988 , vol. 110, p. 8477
反应条件
1: 99.3 percent / NaOMe / methanol / 64 h / Ambient temperature 2: 1.) LiAlH4; 2.) 1N aq. HCl / 1.) THF, 0 deg C, 2.) r.t., 1 h View Scheme
参考文献
Tetrahedron, , vol. 42, # 14 p. 4035 - 4044
