4,4-二甲氧基二苯基甲烷合成路线 （共 148 条）
反应条件
1: diethyl ether; aqueous KI / Erwaermen des Reaktionsprodukts mit wss. Aethanol und Natriumcyanid
2: aqueous H2SO4
View Scheme
参考文献
Kondo; Oshima
Yakugaku Zasshi, 1931 , vol. 51, p. 979,981; dtsch. Ref. S. 131
Chem. Zentralbl., 1932 , vol. 103, # I p. 1894
反应条件
1: AlCl3; CS2 / Behandeln des Reaktionsprodukts mit wss.-aethanol. NaOH und anschliessend mit Dimethylsulfat und wss.-methanol. NaOH
2: N2H4; NaOH
View Scheme
参考文献
Traverso
Gazzetta Chimica Italiana, 1957 , vol. 87, p. 76,87
反应条件
1: AlCl3; CS2 / Behandeln des Reaktionsprodukts mit wss.-aethanol. NaOH und anschliessend mit Dimethylsulfat und wss.-methanol. NaOH
2: N2H4; NaOH
View Scheme
参考文献
Traverso
Gazzetta Chimica Italiana, 1957 , vol. 87, p. 76,87
反应条件
toluene-4-sulfonic acid
参考文献
Bethell, Donald; Hare, Gerard J.; Kearney, Paul A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1981 , p. 684 - 691
反应条件
triethylsilane; trifluorormethanesulfonic acid in chloroform
T=60°C; 15 h; Product distribution; Further Variations:Temperatures;
参考文献
Waterlot; Couturier; De Backer; Rigo
Canadian Journal of Chemistry, 2000 , vol. 78, # 9 p. 1242 - 1246
反应条件
in dichloromethane
Kinetics; byproducts: GePh3CF3, TiCl4; at -70°C;
参考文献
Mayr, Herbert; Basso, Nils
Angewandte Chemie, 1992 , vol. 104, # 8 p. 1103 - 1105
反应条件
in dichloromethane
Kinetics; byproducts: GePh3Cl, TiCl4; at -70°C;
参考文献
Mayr, Herbert; Basso, Nils
Angewandte Chemie, 1992 , vol. 104, # 8 p. 1103 - 1105
反应条件
in dichloromethane
Kinetics; byproducts: GePh3CF3; at -70°C;
参考文献
Mayr, Herbert; Basso, Nils
Angewandte Chemie, 1992 , vol. 104, # 8 p. 1103 - 1105
反应条件
in dichloromethane
Kinetics; byproducts: GePh3Cl, TiCl4; at -70°C;
参考文献
Mayr, Herbert; Basso, Nils
Angewandte Chemie, 1992 , vol. 104, # 8 p. 1103 - 1105
反应条件
in dichloromethane
Kinetics; byproducts: GePh3CF3, TiCl4; at -70°C;
参考文献
Mayr, Herbert; Basso, Nils
Angewandte Chemie, 1992 , vol. 104, # 8 p. 1103 - 1105
