4,4-二甲氧基二苯基甲烷合成路线 （共 148 条）
反应条件
digallium tetrachloride in carbon disulfide
48 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Hashimoto, Yukihiko; Hirata, Kazujuki; Kagoshima, Hirotaka; Kihara, Nobuhiro; Hasegawa, Masaki; Saigo, Kazuhiko
Tetrahedron, 1993 , vol. 49, # 27 p. 5969 - 5978
反应条件
magnesium
T=600°C; P=0.01 - 0.1 Torr; Further byproducts given. Title compound not separated from byproducts;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415
反应条件
1: thionyl chloride / dichloromethane
2: N,N-dimethyl acetamide / 25 °C
View Scheme
参考文献
Streidl, Nicolas; Mayr, Herbert
European Journal of Organic Chemistry, 2011 , # 13 p. 2498 - 2506
反应条件
sodium methylate
T=70°C; C-anode, Pt-cathode, 4.4 F/mol, constant current 0.2 A, undivided cell;
参考文献
Chiba, Toshiro; Okimoto, Mitsuhiro; Nagai, Hiroshi; Takata, Yoshiyuki
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 2968 - 2972
反应条件
methyltrioxorhenium (VII) in benzene
48 h; Ambient temperature; Yield given;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of Organic Chemistry, 1996 , vol. 61, # 1 p. 324 - 328
反应条件
iodine; benzoic acid
T=25°C; 1 h;
参考文献
Jereb, Marjan; Vrazic, Dejan; Zupan, Marko
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2347 - 2352
反应条件
palladium 10 on activated carbon; hydrogen in methanol
2 h;
参考文献
Petursson, Sigthor
Tetrahedron Asymmetry, 2009 , vol. 20, # 6-8 p. 887 - 891
反应条件
Sn(2+)*H(1+)*PW12O40(3-)=SnHPW12O40
T=120°C; 0.5 h;
参考文献
Ramesh Kumar, Ch.; Rao, K.T. Venkateswara; Sai Prasad; Lingaiah
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 337, # 1-2 p. 17 - 24
反应条件
anhydrous iron chloride in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Qian, Xin; Kozak, Christopher M.
Synlett, 2011 , # 6 p. 852 - 856
反应条件
1: 82 percent / triethylamine / ethane-1,2-diol / 0.25 h / Heating
2: 87 percent / 1 h / 20 °C
View Scheme
参考文献
Das, Suven; Froehlich, Roland; Pramanik, Animesh
Journal of Chemical Research, 2006 , # 2 p. 84 - 86
