1-苯甲基-3-苯基-2-硫代脲合成路线 （共 24 条）
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
1: With triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in N,N-dimethyl-formamide
2: With sodium azide in N,N-dimethyl-formamide
T=20°C; 3 h;
参考文献
Chaudhari, Pramod S.; Pathare, Sagar P.; Akamanchi, Krishnacharaya G.
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 3716 - 3723
反应条件
1: acetone / 9 h / Heating
2: hydrazine, conc. HCl / ethanol / 5 h / Heating
3: 86 percent / conc. HCl, NaNO2, K2CO3 / H2O / 4.5 h
4: 92 percent / xylene / 2 h / Heating
5: NaNO2, HCl / H2O
View Scheme
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
反应条件
1: acetone / 9 h / Heating
2: hydrazine, conc. HCl / ethanol / 5 h / Heating
3: 86 percent / conc. HCl, NaNO2, K2CO3 / H2O / 4.5 h
4: 92 percent / xylene / 2 h / Heating
5: NaNO2, HCl / H2O
View Scheme
参考文献
Atherton; Lambert
Tetrahedron, 1983 , vol. 39, # 15 p. 2599 - 2608
