2,2-二甲基-5-异亚丙基-1,3-二噁烷-4,6-二酮合成路线 (共 13 条)
反应条件
1: With ethylenediamine diacetic acid in ethanol
T=20°C; Knoevenagel condensation;
2: With Me2NH*BH3 in ethanol
参考文献
Snider, Barry B.; Smith, Rachel B.
Tetrahedron, 2002 , vol. 58, # 1 p. 25 - 34
反应条件
pyridine; titanium tetrachloride in tetrahydrofuran
21 h; Ambient temperature;
参考文献
Browne, Neil R.; Brown, Roger F. C.; Eastwood, Frank W.; Fallon, Gary D.
Australian Journal of Chemistry, 1987 , vol. 40, # 10 p. 1675 - 1686
反应条件
potassium carbonate
1.) DMF, 1 h, 2.) DMF, 6 h; Yield given. Multistep reaction;
参考文献
Kumbhar, Pramod P; Salunkhe, Manikarao, M; Mane, Ramchandra B
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 9 p. 891