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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
72653-21-5
合成路线
（共 9 条）
865-49-6
氘代氯仿
+
72653-21-5
→
反应条件
33685-54-0
1,1,2,2-四氯乙烷-d2
+
1665-01-6
二氯甲烷-d
+
67311-98-2
+
75-07-0
乙醛
+
75-36-5
乙酰氯
反应条件
T=19.9°C; 0.333333 h; Irradiation; Mechanism;
参考文献
Magnetic Resonance in Chemistry, , vol. 27, # 5 p. 451 - 454
865-49-6
氘代氯仿
+
72653-21-5
→
反应条件
33685-54-0
1,1,2,2-四氯乙烷-d2
+
1665-01-6
二氯甲烷-d
+
67311-98-2
+
75-07-0
乙醛
+
75-36-5
乙酰氯
反应条件
T=19.9°C; 0.333333 h; Irradiation; Mechanism;
参考文献
Zhang, Mao-Xi; Liu, Zhong-Li; Wu, Lung-Min; Liu, You-Cheng
Magnetic Resonance in Chemistry, 1989 , vol. 27, # 5 p. 451 - 454
865-49-6
氘代氯仿
+
72653-21-5
→
反应条件
33685-54-0
1,1,2,2-四氯乙烷-d2
+
1665-01-6
二氯甲烷-d
+
67311-98-2
+
75-07-0
乙醛
+
75-36-5
乙酰氯
反应条件
T=19.9°C; 0.333333 h; Irradiation; Mechanism;
参考文献
Zhang, Mao-Xi; Liu, Zhong-Li; Wu, Lung-Min; Liu, You-Cheng
Magnetic Resonance in Chemistry, 1989 , vol. 27, # 5 p. 451 - 454
72653-21-5
→
反应条件
17159-79-4
对环己酮甲酸乙酯
反应条件
sodium ethanolate
参考文献
Helvetica Chimica Acta, , vol. 62, p. 2802 - 2816
72653-21-5
→
反应条件
20277-40-1
反应条件
1: methanol 2: H2O/KOH / ethanol / 16 h / Ambient temperature 3: hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating 4: 91 percent / concn H2SO4 / 1,2-dichloro-ethane / 20 h / Heating 5: 92 percent / BF3*OEt2 / Ambient temperature 6: 94 percent / NaOMe / methanol / 2 h / Heating 7: 92 percent / SF4 / 24 h / Ambient temperature 8: 96 percent / H2O/KOH / ethanol / 16 h / Ambient temperature 9: 90 percent / diethyl ether; hexane / 2 h / Heating 10: 77 percent / m-chloroperbenzoic acid / CH2Cl2 / 72 h / Ambient temperature 11: 93 percent / NaOMe / methanol / 2 h / Heating 12: 81 percent / SF4 / 24 h / Ambient temperature View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2951 - 2957
72653-21-5
→
反应条件
23062-53-5
4-羟基双环[2.2.2]辛烷-1-羧酸甲酯
反应条件
1: methanol 2: H2O/KOH / ethanol / 16 h / Ambient temperature 3: hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating 4: 91 percent / concn H2SO4 / 1,2-dichloro-ethane / 20 h / Heating 5: 92 percent / BF3*OEt2 / Ambient temperature 6: 94 percent / NaOMe / methanol / 2 h / Heating View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2951 - 2957
72653-21-5
→
反应条件
773-34-2
反应条件
1: methanol 2: H2O/KOH / ethanol / 16 h / Ambient temperature 3: hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2951 - 2957
865-49-6
氘代氯仿
+
72653-21-5
→
反应条件
33685-54-0
1,1,2,2-四氯乙烷-d2
+
1665-01-6
二氯甲烷-d
+
67311-98-2
+
75-07-0
乙醛
+
75-36-5
乙酰氯
反应条件
T=19.9°C; 0.333333 h; Irradiation; Mechanism;
参考文献
Zhang, Mao-Xi; Liu, Zhong-Li; Wu, Lung-Min; Liu, You-Cheng
Magnetic Resonance in Chemistry, 1989 , vol. 27, # 5 p. 451 - 454
72653-21-5
→
反应条件
81687-78-7
4-氟双环[2.2.2]辛烷-1-甲酰氯
反应条件
1: methanol 2: H2O/KOH / ethanol / 16 h / Ambient temperature 3: hydrazine hydrate, KOH / bis-(2-hydroxy-ethyl) ether / 10 h / Heating 4: 91 percent / concn H2SO4 / 1,2-dichloro-ethane / 20 h / Heating 5: 92 percent / BF3*OEt2 / Ambient temperature 6: 94 percent / NaOMe / methanol / 2 h / Heating 7: 92 percent / SF4 / 24 h / Ambient temperature 8: 96 percent / H2O/KOH / ethanol / 16 h / Ambient temperature 9: thionyl chloride View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2951 - 2957
