(+)-乙基 (R)-3-羟基-3-苯丙酸盐合成路线 （共 53 条）
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
Candida rugose type VII lipase in octane T=20°C; 15 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
sodium hydroxide; Pseudomonas candida lipase in phosphate buffer T=20°C; resolution of racemate; pH=7.0; 24 h; ultrasound; Product distribution; Further Variations:pH-valuesReagentsmagnetic stirring;
参考文献
Ribeiro, Carlos Magno R.; Passaroto, Elisa N.; Brenelli, Eugenia C.S.
Tetrahedron Letters, 2001 , vol. 42, # 37 p. 6477 - 6479
反应条件
1: TiCl4 / CH2Cl2 / -78 °C 2: pyridinium chlorochromate / CH2Cl2 / Ambient temperature 3: Amberlyst A26 CO3(2-) form / benzene / 50 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 9 p. 596 - 597
反应条件
1: pyridinium chlorochromate / CH2Cl2 / Ambient temperature 2: Amberlyst A26 CO3(2-) form / benzene / 50 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 9 p. 596 - 597
反应条件
1: Candida rugose type VII lipase; water / di-isopropyl ether / 15 h / 20 °C / Enzymatic reaction 2: Candida rugose type VII lipase; water / di-isopropyl ether / 20 °C / Enzymatic reaction View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
1: zinc / tetrahydrofuran / 1.5 h / |Reflux 2: cobalt(II) chloride / acetonitrile / 8 h / |Reflux 3: Saccharomyces cerrvisatae (ATCC 9080) / water / 48 h / 20 °C / |Enzymatic reaction View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 24, # 21-22 p. 1389 - 1394
反应条件
1: Cu(OH)2; (S, S)-6,6’-bis(1-hydroxy-2,2-dimethylpropyl)-2,2’-bipyridine; acetic acid / water / 12 h / 5 °C 2: sodium peroxoborate tetrahydrate / 4 h / 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 51 p. 12763 - 12766
Angew. Chem., , vol. 124, # 51 p. 12935 - 12938
反应条件
1: sodium tetrahydroborate / ethanol / 2 h / 20 °C 2: cobalt(II) chloride / acetonitrile / 8 h / |Reflux 3: Saccharomyces cerrvisatae (ATCC 9080) / water / 48 h / 20 °C / |Enzymatic reaction View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 24, # 21-22 p. 1389 - 1394
