(-)-甲基-D-BATA-羟基异丁酸酯合成路线 （共 18 条）
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; (Rc,Ra)-THNAPhos; hydrogen in dichloromethane T=20°C; P=7500.75 Torr; 24 h; optical yield given as percent ee;
参考文献
Tetrahedron Asymmetry, , vol. 20, # 2 p. 210 - 213
反应条件
hydrogen; [(R,R)-Me-DuPhosRhCOD] triflate in methanol T=30°C; P=3000.3 Torr; Product distribution; Further Variations:Catalysts;
参考文献
Advanced Synthesis and Catalysis, , vol. 345, # 1-2 p. 185 - 189
反应条件
[Rh(dppb)(COD)]BF4; hydrogen in methanol T=20°C; P=45004.5 Torr; 20 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 16 p. 2533 - 2543
参考文献
Choy, William; Ma, Philip; Masamune, Satoru
Tetrahedron Letters, 1981 , vol. 22, # 37 p. 3555 - 3556
反应条件
in diethyl ether Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 47, # 12 p. 2400 - 2404
反应条件
TEA; diisobutylaluminium hydride; 4-(N,N-dimethlyamino)pyridine 2) CH2Cl2, -78 deg C; Multistep reaction;
参考文献
Kraft, Philip; Tochtermann, Werner
Liebigs Annalen der Chemie, 1994 , # 12 p. 1161 - 1164
反应条件
α,α,α-trifluorotoluene; magnesium oxide T=83°C; 24 h;
参考文献
Poon, Kevin W. C.; Dudley, Gregory B.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3923 - 3927
反应条件
magnesium oxide in various solvent(s) T=0 - 20°C;
参考文献
Nwoye, Ernest O.; Dudley, Gregory B.
Chemical Communications, 2007 , # 14 p. 1436 - 1437
反应条件
α,α,α-trifluorotoluene; magnesium oxide T=83°C; 24 h;
参考文献
Poon, Kevin W. C.; Dudley, Gregory B.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3923 - 3927
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=5°C; Etherification; silylation;
参考文献
Cooksey, John P.; Ford, Rhonan; Kocienski, Philip J.; Pelotier, Beatrice; Pons, Jean-Marc
Tetrahedron, 2010 , vol. 66, # 33 p. 6462 - 6467
