4-甲氧基苯并[d]噻唑-2-甲腈合成路线 （共 5 条）
反应条件
1: HCl
2: NH3 / methanol
3: POCl3 / Heating
View Scheme
参考文献
White,E.H.; Woerther,H.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1484 - 1488
反应条件
1: NH3 / methanol
2: POCl3 / Heating
View Scheme
参考文献
White,E.H.; Woerther,H.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1484 - 1488
反应条件
trichlorophosphate
Heating;
参考文献
White,E.H.; Woerther,H.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1484 - 1488
反应条件
1: 2.) pyridine / 1) CH2Cl2, rt, 2 h; 2) CH2Cl2, rt, 2 h
2: 52 percent / 0.07 h / 150 - 160 °C / microwave irradiation at 300 W; further conditions: thermolysis
View Scheme
参考文献
Beneteau, Valerie; Besson, Thierry; Rees, Charles W.
Synthetic Communications, 1997 , vol. 27, # 13 p. 2275 - 2280
反应条件
pyridine hydrochloride
参考文献
White,E.H.; Woerther,H.
Journal of Organic Chemistry, 1966 , vol. 31, p. 1484 - 1488
