4-氰基-2,6-二甲氧基苯酚合成路线 （共 7 条）
反应条件
sodium azide; trifluorormethanesulfonic acid in acetonitrile
T=20°C; Schmidt reaction; 0.0333333 h;
参考文献
Rokade, Balaji V.; Prabhu, Kandikere Ramaiah
Journal of Organic Chemistry, 2012 , vol. 77, # 12 p. 5364 - 5370
反应条件
2-(N,N-diethylamino)ethanethiol hydrochloride; sodium t-butanolate in N,N-dimethyl-formamide
0.8 h; Heating;
参考文献
Magano, Javier; Chen, Michael H.; Clark, Jerry D.; Nussbaumer, Thomas
Journal of Organic Chemistry, 2006 , vol. 71, # 18 p. 7103 - 7105
反应条件
phthalic anhydride
0.0833333 h; Heating;
参考文献
Wang, Eng-Chi; Huang, Keng-Shiang; Chen, Hsing-Ming; Wu, Chung-Chin; Lin, Gwo-Jiun
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 3 p. 619 - 627
反应条件
dihydrogen peroxide in formic acid; water
T=40°C; 0.0666667 h;
参考文献
Orita, Hideo; Shimizu, Masao; Hayakawa, Takashi; Takehira, Katsuomi
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 5 p. 1652 - 1657
反应条件
hydrogenchloride; diethyl ether
参考文献
McCord
Journal of the American Chemical Society, 1931 , vol. 53, p. 4181
反应条件
1: 92 percent / CuBr / dimethylformamide
2: 77 percent / NH2OH*HCl; CH3CO2Na/HCO2H
View Scheme
参考文献
Zabinski, Jerzy; Wolska, Irena; Maciejewska, Dorota
Journal of Molecular Structure, 2007 , vol. 833, # 1-3 p. 74 - 81
反应条件
1: 97 percent / Br2 / methanol
2: 92 percent / CuBr / dimethylformamide
3: 77 percent / NH2OH*HCl; CH3CO2Na/HCO2H
View Scheme
参考文献
Zabinski, Jerzy; Wolska, Irena; Maciejewska, Dorota
Journal of Molecular Structure, 2007 , vol. 833, # 1-3 p. 74 - 81
