2-(三氟甲基)苯并苯酮合成路线 （共 19 条）
反应条件
aluminium trichloride T=0 - 2°C; 2 h;
参考文献
Bulletin de la Societe Chimique de France, , p. 587 - 593
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 2 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 68, # 13 p. 5236 - 5243
反应条件
1.1: tert.-butylnitrite / water; ethanol / 1 h / 0 - 20 °C / |Inert atmosphere 2.1: copper(I) isothiocyanate; caesium carbonate / acetonitrile / 0.17 h / 20 °C / |Inert atmosphere 2.2: 16 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 7972 - 7975
Angew. Chem., , vol. 125, # 31 p. 8130 - 8133
反应条件
silver(I) acetate; potassium; carbon; lithium chloride; zinc(II) chloride 1.) 160 deg C, 15 min, 2.) THF, 25 deg C, 3.) THF, -60 deg C, 4.) -10 deg C, 14 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 7 p. 1047 - 1050
反应条件
1: SOCl2 2: AlCl3 / 2 h / 0 - 2 °C View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 587 - 593
参考文献
Arzneimittel Forschung, , vol. 14, p. 964 - 967
反应条件
sodium hydroxide; zinc in ethanol 2 h; Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 587 - 593
反应条件
n-butyl-magnesium bromide in diethyl ether T=0°C; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 7 p. 2573 - 2575
反应条件
in diethyl ether T=0°C; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 56, # 7 p. 2573 - 2575
