5-重氮米氏酸(=5-重氮-2,2-二甲基-1,3-二氧杂环己烷-4,6-二酮)合成路线 （共 27 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; 4-toluenesulfonyl azide; triethylamine 3 h; Ambient temperature;
参考文献
Benati, Luisa; Montevecchi, P. Carlo; Spagnolo, Piero
Gazzetta Chimica Italiana, 1992 , vol. 122, # 5-7 p. 249 - 251
反应条件
in dichloromethane 4 h; Heating;
参考文献
Kokel, Bruno; Viehe, Heinz Guenter
Angewandte Chemie, 1980 , vol. 92, # 9 p. 754 - 755
反应条件
in toluene 2 h; Heating;
参考文献
Heterocycles, , vol. 46, # 1 p. 503 - 508
反应条件
T=20°C; 1.1 h; UV-irradiation;
参考文献
Tetrahedron Letters, , vol. 46, # 3 p. 435 - 438
反应条件
in toluene 2 h; Heating; Product distributionMechanism;
参考文献
Heterocycles, , vol. 46, # 1 p. 503 - 508
反应条件
UV-irradiation; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 125, # 46 p. 14153 - 14162
反应条件
in chloroform-d1 T=50°C; KineticsProduct distribution; Further Variations:Solventsirradiation;
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 8 p. 1213 - 1219
反应条件
1: 18 percent / tetrahydrofuran / 2 h / 18 - 20 °C / UV-irradiation 2: 46 percent / tetrahydrofuran / 1.8 h / 18 - 20 °C / UV-irradiation View Scheme
参考文献
Nikolaev; Shevchenko; Platz; Khimich
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 6 p. 815 - 827
反应条件
in tetrahydrofuran; water 3.5 h; Irradiation; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 3 p. 264 - 268
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 3 p. 321 - 325
反应条件
in tetrahydrofuran; water 3.5 h; Irradiation; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 21, # 3 p. 264 - 268
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 21, # 3 p. 321 - 325
