2-氯-3-氰基-6-甲基-5-硝基异烟酸乙酯合成路线 （共 10 条）
反应条件
phosphorus pentachloride; chlorobenzene
参考文献
Scientific Papers of the Institute of Physical and Chemical Research (Japan), , vol. 38, p. 347,350
反应条件
1: HNO3, / acetic anhydride 2: PCl3 / chlorobenzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 8 p. 1809 - 1817
反应条件
1: Et2NH 2: HNO3, / acetic anhydride 3: PCl3 / chlorobenzene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 8 p. 1809 - 1817
反应条件
1: palladium/BaCO3; ethanol / 36775.4 - 44130.5 Torr / Hydrogenation
2: concentrated aqueous HCl
3: aqueous H2SO4; aqueous NaNO2 / 90 - 95 °C
4: ethanol / Erhitzen des vom Aethanol befreiten Reaktionsgemisches auf 115-125grad
5: lithium alanate; diethyl ether / 0 °C
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
反应条件
palladium-barium carbonate; ethanol
P=760 Torr; Hydrogenation;
参考文献
Pieper; Yang; Zhou; Liu
Journal of the American Chemical Society, 1997 , vol. 119, # 8 p. 1809 - 1817
反应条件
ethanol; platinum
Hydrogenation;
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
Full Text Show Details
Velluz; Amiard
Bulletin de la Societe Chimique de France, 1947 , p. 136,139
反应条件
1: SnCl2; concentrated aqueous HCl; acetic acid
2: palladium/BaSO4; ethanol / Hydrogenation
3: concentrated aqueous HCl
4: aqueous H2SO4; aqueous NaNO2 / 90 - 95 °C
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
反应条件
1: palladium/BaCO3; ethanol / 36775.4 - 44130.5 Torr / Hydrogenation
2: concentrated aqueous HCl
3: aqueous H2SO4; aqueous NaNO2 / 90 - 95 °C
4: diethyl ether; methanol / -15 °C
5: lithium alanate; diethyl ether / 0 °C
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
反应条件
1: palladium/BaCO3; ethanol / 760 Torr / Hydrogenation
2: Raney nickel; ethanol / Hydrogenation
View Scheme
参考文献
Velluz; Amiard
Bulletin de la Societe Chimique de France, 1947 , p. 136,139
反应条件
1: SnCl2; concentrated aqueous HCl; acetic acid
2: palladium/BaSO4; ethanol / Hydrogenation
3: concentrated aqueous HCl
View Scheme
参考文献
Wuest et al.
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 226,240
