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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
八倾吲嗪三醇
合成路线
（共 265 条）
94349-19-6
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
Dowex 50W-X8 in methanol 24 h;
参考文献
Adams, Curtis E.; Walker, Frederick J.; Sharpless, K. Barry
Journal of Organic Chemistry, 1985 , vol. 50, # 3 p. 420 - 422
1002754-03-1
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: DMAP / CH2Cl2 / -78 °C 2: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C 3: NaBH4 / CH2Cl2; methanol / -78 °C 4: pyridine; DMAP / CH2Cl2 / 20 °C 5: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 6: TBAF / tetrahydrofuran / 20 °C 7: triethylamine / CH2Cl2 8: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 9: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
886852-69-3
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: NBS; H2O; NaHCO3 / NaOAc*3H2O / tetrahydrofuran / 0 °C 2: DMAP / CH2Cl2 / -78 °C 3: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C 4: NaBH4 / CH2Cl2; methanol / -78 °C 5: pyridine; DMAP / CH2Cl2 / 20 °C 6: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 7: TBAF / tetrahydrofuran / 20 °C 8: triethylamine / CH2Cl2 9: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 10: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
1002754-27-9
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C 2: NaBH4 / CH2Cl2; methanol / -78 °C 3: pyridine; DMAP / CH2Cl2 / 20 °C 4: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 5: TBAF / tetrahydrofuran / 20 °C 6: triethylamine / CH2Cl2 7: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 8: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
1002754-04-2
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: NaBH4 / CH2Cl2; methanol / -78 °C 2: pyridine; DMAP / CH2Cl2 / 20 °C 3: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 4: TBAF / tetrahydrofuran / 20 °C 5: triethylamine / CH2Cl2 6: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 7: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
1002754-01-9
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: TBAF / tetrahydrofuran / 20 °C 2: triethylamine / CH2Cl2 3: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 4: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
1002754-11-1
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 2: TBAF / tetrahydrofuran / 20 °C 3: triethylamine / CH2Cl2 4: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 5: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
120853-04-5
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: 98 percent / imidazole / dimethylformamide / 0 - 20 °C 2: formic acid; triethylamine / Ru(η6-mesitylene)-(R,R)-TsDPEN / CH2Cl2 / 20 °C 3: NBS; H2O; NaHCO3 / NaOAc*3H2O / tetrahydrofuran / 0 °C 4: DMAP / CH2Cl2 / -78 °C 5: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C 6: NaBH4 / CH2Cl2; methanol / -78 °C 7: pyridine; DMAP / CH2Cl2 / 20 °C 8: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 9: TBAF / tetrahydrofuran / 20 °C 10: triethylamine / CH2Cl2 11: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 12: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
691870-87-8
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: formic acid; triethylamine / Ru(η6-mesitylene)-(R,R)-TsDPEN / CH2Cl2 / 20 °C 2: NBS; H2O; NaHCO3 / NaOAc*3H2O / tetrahydrofuran / 0 °C 3: DMAP / CH2Cl2 / -78 °C 4: Pd2(DBA)3*CHCl3; triphenylphosphine / CH2Cl2 / 0 - 20 °C 5: NaBH4 / CH2Cl2; methanol / -78 °C 6: pyridine; DMAP / CH2Cl2 / 20 °C 7: TMSN3 / allylpalladium chloride dimer; 1,4-bis(diphenylphosphino)butane / tetrahydrofuran / 50 °C 8: TBAF / tetrahydrofuran / 20 °C 9: triethylamine / CH2Cl2 10: N-methylmorpholine N-oxide; water / OsO4 / 2-methyl-propan-2-ol; acetone 11: H2 / Pd(OH)2/C / ethanol / 20 °C / 5171.48 Torr View Scheme
参考文献
Organic Letters, , vol. 8, # 8 p. 1609 - 1612
476171-47-8
→
反应条件
72741-87-8
八倾吲嗪三醇
反应条件
1: 77 percent / Et3N / CH2Cl2 / 2 h / 0 °C 2: 77 percent / (benzylidene)bis(tricyclohexylphosphine)dichlororuthenium / CH2Cl2 / 18 h / Heating 3: K2OsO4*2H2O; N-methylmorpholine oxide; pyridine / acetone; H2O / 168 h / 20 °C 4: 100 percent / NaH; tetrabutylammonium iodide / tetrahydrofuran / 48 h / 20 °C 5: 83.7 percent / NaOH / methanol; H2O / 2 h / 110 °C / microwave irradiation 6: 96.9 percent / imidazole / acetonitrile / 72 h / 65 °C 7: 91.8 percent / cerium(IV) ammonium nitrate / acetonitrile; H2O / 3 h / 20 °C 8: 93.4 percent / CBr4; PPh3; Et3N / CH2Cl2 / 0 - 4 °C 9: 75.8 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 120 h / 20 °C 10: 93 percent / H2; PdCl2 / methanol / 2 h / 20 °C / 760 Torr View Scheme
参考文献
Australian Journal of Chemistry, , vol. 57, # 7 p. 669 - 672
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