反应条件
1: 100 percent / LiAlH4 / tetrahydrofuran / Ambient temperature 2: 100 percent / tetrahydrofuran; H2O / 0 °C 3: 95 percent / pyridine / 0 °C 4: TsOH / methanol; H2O / 72 h / Ambient temperature 5: amberlite IRA-400/OH(1-) 6: Collins reagent / CH2Cl2 / 5 °C 7: tetrahydrofuran / 0 °C 8: 58 percent / NaBH4 / ethanol; various solvent(s) / 1 h / Heating 9: H2, 10percent Pd/C / ethanol / 1551.4 Torr 10: 60 percent / ethanol / Heating 11: 60 percent / NaBH4 / ethanol; tetrahydrofuran / Heating 12: 75 percent / 6N HCl / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 20 p. 3948 - 3950
