N,N'-二氧化-2,2'-联吡啶合成路线 （共 27 条）
反应条件
1: 16 percent / KNO3; H2SO4 / 24 h / 100 °C 2: 64 percent / CH3COBr; glacial AcOH / 2 h / Heating 3: 60 percent / PBr3 / CHCl3 / 1.25 h / Heating View Scheme
参考文献
Zhu, Sherry S.; Kingsborough, Richard P.; Swager, Timothy M.
Journal of Materials Chemistry, 1999 , vol. 9, # 9 p. 2123 - 2131
反应条件
1: 52 percent / HNO3; H2SO4/SO3 / 8 h / 100 °C 2: 67 percent / NaOMe / 5 h / 30 - 35 °C 3: 60 percent / PCl3 / CHCl3 / 5 h / Heating View Scheme
参考文献
Ten Brink, Gerd-Jan; Arends, Isabel W. C. E.; Hoogenraad, Marcel; Verspui, Goeran; Sheldon, Roger A.
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 4 p. 497 - 505
反应条件
1: 90percent HNO3; 30percent SO3 / H2SO4 / 110 °C 2: AcBr / acetic acid / Heating 3: PBr3 / CHCl3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 47 p. 14162 - 14172
反应条件
1: 52 percent / HNO3; H2SO4/SO3 / 8 h / 100 °C 2: 80 percent / AcCl; AcOH / 4 h / 100 °C 3: 86 percent / PCl3 / acetonitrile / 6 h / Heating View Scheme
参考文献
Murase
Nippon Kagaku Zasshi, 1956 , vol. 77, p. 682,685
Chem.Abstr., 1958 , p. 9100
反应条件
trichlorophosphate 5 h; Heating;
参考文献
Tetrahedron, , vol. 39, # 2 p. 291 - 296
反应条件
1: 52 percent / HNO3; H2SO4/SO3 / 8 h / 100 °C
2: 80 percent / AcCl; AcOH / 4 h / 100 °C
View Scheme
参考文献
Anderson, Susan; Constable, Edwin C.; Seddon, Kenneth R.; Turp, Janet E.; Baggott, James E.; Pilling, Michael J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1985 , p. 2247 - 2262
反应条件
1: 90percent HNO3; 30percent SO3 / H2SO4 / 110 °C
2: AcBr / acetic acid / Heating
View Scheme
参考文献
SFC CO., LTD.
Patent: US2012/247546 A1, 2012 ;
反应条件
trichlorophosphate
5 h; Heating;
参考文献
Constable, Edwin C.; Seddon, Kenneth R.
Tetrahedron, 1983 , vol. 39, # 2 p. 291 - 296
反应条件
1: sulfuric acid; nitric acid / 4 h / 95 °C / |Inert atmosphere; |Schlenk technique
2: acetic acid; acetyl chloride / 4 h / 100 °C / |Inert atmosphere; |Schlenk technique
3: trichlorophosphate / chloroform / 19 h / |Inert atmosphere; |Reflux; |Schlenk technique
4: 90 h / 200 - 220 °C / |Sealed tube; |Inert atmosphere; |Schlenk technique
View Scheme
参考文献
Ladouceur, Sebastien; Swanick, Kalen N.; Gallagher-Duval, Shawn; Ding, Zhifeng; Zysman-Colman, Eli
European Journal of Inorganic Chemistry, 2013 , # 30 p. 5329 - 5343
反应条件
benzoyl chloride in dichloromethane
T=20°C;
参考文献
Andreiadis, Eugen S.; Demadrille, Renaud; Imbert, Daniel; Pecaut, Jacques; Mazzanti, Marinella
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9458 - 9476
