1-(7-甲氧基-2-萘)-乙酮合成路线 (共 4 条)
反应条件
3 A molecular sieve; oxygen; sodium carbonate; Pd((-)-sparteine)2Cl2 in tert-butyl alcohol
T=65°C; 24 h; Title compound not separated from byproducts;
参考文献
Mandal, Sunil K.; Sigman, Matthew S.
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7535 - 7537
反应条件
1: 75 percent / DIPEA / Pd2(dba)3; 1,1'-bis(diphenylphosphino)ferrocene / dioxane / 1.25 h / 85 °C
2: 63 mg / aq. HCl / dioxane / 1 h / 20 °C
View Scheme
参考文献
Hansen, Anders Lindhardt; Skrydstrup, Troels
Journal of Organic Chemistry, 2005 , vol. 70, # 15 p. 5997 - 6003
反应条件
1: DDQ
2: (alkaline hydrolysis)
View Scheme
参考文献
Tsuno,Y. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 3033 - 3042
参考文献
Tsuno,Y. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, p. 3033 - 3042