6-苯氨基-1,3-二甲基尿嘧啶合成路线 （共 6 条）
反应条件
sodium nitrite in acetic acid T=25 - 30°C; 0.666667 h; Yields of byproduct given;
参考文献
Krasnov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 1 p. 115 - 119
反应条件
in dichloromethane 2 h; Ambient temperaturethen refluxed for 2-3 h;
参考文献
Kokel; Boussouira
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 6 p. 1493 - 1498
反应条件
1: 85 percent / diphenyl ether / 2 h / 220 - 250 °C 2: 75 percent / POCl3 / 50 - 60 °C View Scheme
参考文献
Khattab, Ahmed F. A.; Van Tinh, Dang; Stadlbauer, Wolfgang
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 2 p. 151 - 156
反应条件
sodium nitrite in acetic acid
T=25 - 30°C; 0.666667 h; Yields of byproduct given;
参考文献
Krasnov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 1 p. 115 - 119
反应条件
acetic acid; zinc; sodium nitrite
1.) AcOH, 25-30 deg C, 40 min, 2.) 100 deg C, 20 min; Yield givenMultistep reaction;
参考文献
Krasnov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 1 p. 115 - 119
反应条件
in dichloromethane
2 h; Ambient temperaturethen refluxed for 2-3 h;
参考文献
Kokel; Boussouira
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 6 p. 1493 - 1498
