反应条件
1: trichlorophosphate / 1,2-dichloro-ethane / 8 h / 60 °C
2: potassium tert-butylate / 2-methyl tetrahydrofuran / 9 h / Inert atmosphere; Reflux
3: pyridine / dichloromethane / 1 h / -78 °C
4: dimethylsulfone; potassium iodide / N,N-dimethyl-formamide / 1.5 h / 85 °C
View Scheme
参考文献
Ribecai, Arianna; Bacchi, Sergio; Delpogetto, Monica; Guelfi, Simone; Manzo, Angelo Maria; Perboni, Alcide; Stabile, Paolo; Westerduin, Pieter; Hourdin, Marie; Rossi, Sara; Provera, Stefano; Turco, Lucilla
Organic Process Research and Development, 2010 , vol. 14, # 4 p. 895 - 901
