二甲基-4-(三氟甲基)邻苯二甲酸酯合成路线 （共 3 条）
反应条件
1: T=100°C; Diels-Alder cycloaddition; 16 h;
2: With potassium carbonate in acetone
1 h; Heating; Further stages.;
参考文献
Volle, Jean-Noel; Schlosser, Manfred
European Journal of Organic Chemistry, 2002 , # 9 p. 1490 - 1492
反应条件
iodine
T=100°C; 18 h;
参考文献
Schlosser, Manfred; Keller, Holger
Liebigs Annalen, 1995 , # 9 p. 1587 - 1590
反应条件
1: sodium dithionite; Na3PO4*12H2O / acetonitrile; water / 48 h / -78 - 20 °C
2: potassium carbonate / dimethyl sulfoxide / 12 h / 60 °C
View Scheme
参考文献
Ponomarenko, Maxim V.; Lummer, Katrin; Fokin, Andrey A.; Serguchev, Yurii A.; Bassil, Bassem S.; Roeschenthaler, Gerd-Volker
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 46 p. 8103 - 8112
