2-溴-1,3-二苯基丙烷-1,3-二酮合成路线 （共 45 条）
反应条件
1: PhCOCHBrCOPh; triethyl phosphite in tetrahydrofuran
T=0°C; 1 h;
2: Ph2Cu(CN)Li2 With boron trifluoride diethyl etherate in tetrahydrofuran; diethyl ether
T=-78°C;
参考文献
Onishi, Jim Yoshitaka; Takuwa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2003 , vol. 32, # 11 p. 994 - 995
反应条件
1: 97 percent / 1-methyl-pyrrolidin-2-one / 48 h / 20 °C
2: 80 percent / phenyl hydrazine / methanol; acetic acid / 24 h / 20 °C
View Scheme
参考文献
Withbroe, Gregory J.; Singer, Robert A.; Sieser, Janice E.
Organic Process Research and Development, 2008 , vol. 12, # 3 p. 480 - 489
参考文献
Blatt
J. Washington Acad., 1938 , vol. 28, p. 1,4
参考文献
Ziemelis,Z. et al.
Doklady Chemistry, 1965 , vol. 164, p. 840 - 843
Doklady Akademii Nauk SSSR, 1965 , vol. 164, p. 106 - 109
反应条件
(i) EtOH, (ii) /BRN= 605631/; Multistep reaction;
参考文献
Ziemelis,Z. et al.
Doklady Chemistry, 1965 , vol. 164, p. 840 - 843
Doklady Akademii Nauk SSSR, 1965 , vol. 164, p. 106 - 109
