4-(三氟甲基)二苯甲酮合成路线 (共 50 条)
反应条件
in acetonitrile 14 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9786 - 9789
反应条件
1.1: hydrogenchloride / water / 0 - 5 °C 1.2: 0.17 h / 5 °C 2.1: acetonitrile / 6 h / 20 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 23 p. 8436 - 8439
参考文献
Cnad. J. Chem., , vol. 33, p. 1633,1634
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 85, p. 367 - 372
反应条件
magnesium 1.) diethyl ether, 4 h, 2.) diethyl ether, room temperature, overnight; Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 58, p. 2537 - 2549
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 54, # 5 p. 699 - 702
反应条件
[(OC-6-13)-RuCl2[P(p-CH3C6H5)3]2(en)]; potassium tert-butylate; hydrogen in isopropyl alcohol; tert-butyl alcohol T=28°C; Catalytic hydrogenation; P=6080.41 Torr; 1 h;
参考文献
Ohkuma, Takeshi; Koizumi, Masatoshi; Ikehira, Hideyuki; Yokozawa, Tohru; Noyori, Ryoji
Organic Letters, 2000 , vol. 2, # 5 p. 659 - 661
反应条件
1: tetrahydrofuran 2: (diacetoxy)iodobenzene; I2 / CH2Cl2 / 0.17 h / 20 °C / Irradiation View Scheme
参考文献
Aureliano Antunes, Carla S.; Bietti, Massimo; Ercolani, Gianfranco; Lanzalunga, Osvaldo; Salamone, Michela
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 3884 - 3891
反应条件
triethylsilane; boron trifluoride diethyl etherate in dichloromethane 10 h; Ambient temperature;
参考文献
Smonou
Synthetic Communications, 1994 , vol. 24, # 14 p. 1999 - 2002
反应条件
1: tetrahydrofuran 2: (diacetoxy)iodobenzene; I2 / CH2Cl2 / 0.17 h / 20 °C / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 10 p. 3884 - 3891