1,1,1,2,3,4,4,5,5,5-十氟戊-2-烯合成路线 (共 7 条)
反应条件
hydrogen; Ni/Cu/Cr/CaF2 T=307 - 425°C; Gas phase; Product distribution / selectivity;
参考文献
WO2009/79525 A2, ;
Page/Page column 14-15 ;
反应条件
cesium fluoride in diethylene glycol dimethyl ether 12 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, # 11 p. 2066 - 2071
Zhurnal Organicheskoi Khimii, , vol. 20, # 11 p. 2267 - 2273
反应条件
fluorine T=20 - 40°C; 0.666667 h; fluorination of perfluoroolefins with elemental fluorine in the gas and liquid phase; heats of fluorination; Product distributionThermodynamic data;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167
反应条件
fluorine T=20 - 40°C; 0.666667 h; fluorination of perfluoroolefins with elemental fluorine in the gas and liquid phase; heats of fluorination; Product distributionThermodynamic data;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167
反应条件
fluorine T=20 - 40°C; 0.666667 h; fluorination of perfluoroolefins with elemental fluorine in the gas and liquid phase; heats of fluorination; Product distributionThermodynamic data;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167
反应条件
fluorine T=20 - 40°C; 0.666667 h; fluorination of perfluoroolefins with elemental fluorine in the gas and liquid phase; heats of fluorination; Product distributionThermodynamic data;
参考文献
Moldavskii, Dmitrii D.; Bispen, Tatjana A.; Kaurova, Galina I.; Furin, Georgii G.
Journal of Fluorine Chemistry, 1999 , vol. 94, # 2 p. 157 - 167
反应条件
sodium hydroxide; sulfuric acid; sulfur trioxide; SbF5 Yield given. Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 34, # 8 p. 1714 - 1718
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 8 p. 1864 - 1868