1,2-O-异亚丙基-5,6-二脱氧-呋喃葡萄糖合成路线 （共 33 条）
反应条件
oxygen in dichloromethane
72 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Kudelska, Wieslawa; Michalska, Maria
Tetrahedron, 1981 , vol. 37, # 17 p. 2989 - 2994
反应条件
1: 87 percent / aq. acetic acid / 24 h / 20 °C
2: 1) Ph3P, imidazole, iodine, 2) aq. NaOH / 1) toluene, 80 deg C, 3 h, 2) methanol, RT, 30 min
View Scheme
参考文献
Tsui, Hon-Chung; Paquette, Leo A.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9968 - 9977
反应条件
in benzene
48 h; Ambient temperature; Yields of byproduct given;
参考文献
Kudelska, Wieslawa; Michalska, Maria
Tetrahedron, 1981 , vol. 37, # 17 p. 2989 - 2994
反应条件
in chloroform-d1
to CDCl3 soln. of Sn compd. was added CF3COOH; detected by (1)H-NMR spectroscopy;
参考文献
Taylor, Oonah J.; Wardell, James L.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 267 - 272
反应条件
in chloroform-d1
byproducts: C6H6; to a soln. of Sn compd. in CDCl3 was added CF3COOH; detected by (1)H-NMR spectroscopy;
参考文献
Taylor, Oonah J.; Wardell, James L.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 267 - 272
反应条件
in chloroform-d1
byproducts: C6H5COOH; to CDCl3 soln. of Sn compd. was added C6H5COCl, react. mixt. was left for 14 d; detected by (1)H-NMR spectroscopy;
参考文献
Taylor, Oonah J.; Wardell, James L.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 267 - 272
反应条件
in chloroform-d1
to CDCl3 soln. of Sn compd. was added ClCO2Et, after 11 d at room temp. was react. ca 50percent complete;
参考文献
Taylor, Oonah J.; Wardell, James L.
Recueil des Travaux Chimiques des Pays-Bas, 1988 , vol. 107, # 3 p. 267 - 272
反应条件
in benzene
3 h; HeatingOther reagents, solvent, temperature; Product distribution;
参考文献
Kudelska, Wieslawa; Michalska, Maria
Tetrahedron, 1981 , vol. 37, # 17 p. 2989 - 2994
参考文献
Jones; Thompson
Canadian Journal of Chemistry, 1957 , vol. 35, p. 955,958
反应条件
sodium hydride in N,N-dimethyl-formamide
1.5 h; Ambient temperature;
参考文献
Krohn, Karsten; Ekkundi, Vadiraj S.; Doering, Detlev; Jones, Peter
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 2 p. 153 - 170
