hydrogenchloride in n-heptane T=95 - 100°C; 3 h; during the reaction was the product continuously extracted with heptane;

1: 94 percent / H2 / copper-chromium catalyst / ethanol / 6 h / 250 °C / 114000 Torr 2: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane View Scheme

1: 93.5 percent / ethanol / 14 h / Heating 2: 94 percent / H2 / copper-chromium catalyst / ethanol / 6 h / 250 °C / 114000 Torr 3: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane View Scheme