1-(2-甲基苯基)乙醇合成路线 （共 64 条）
反应条件
palladium dichloride in methanol T=40°C; 12 h; Inert atmosphereGreen chemistry; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 2-3 p. 341 - 347
反应条件
(1R)-N-oxyl-1-(N-benzylcarbamoyl)-8-azabicyclo[3.2.1]octane; sodium hydrogencarbonate; sodium bromide in dichloromethane; water T=0°C; Electrochemical reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Demizu, Yosuke; Shiigi, Hirofumi; Mori, Hiroyuki; Matsumoto, Kazuya; Onomura, Osamu
Tetrahedron Asymmetry, 2008 , vol. 19, # 23 p. 2659 - 2665
反应条件
chiral 2-(3',5'-di-tert-butylphenyl)-4,4,8-trimethyl-2-phosphabicyclolt;3.3.0gt;octane in n-heptane T=-40°C; 4 h; Title compound not separated from byproducts;
参考文献
Birman, Vladimir B.; Li, Ximin
Organic Letters, 2006 , vol. 8, # 7 p. 1351 - 1354
反应条件
sodium hydrogencarbonate; sodium bromide; chiral azabicyclo-N-oxyl in dichloromethane T=0°C; Electrochemical reaction;
参考文献
Ebner, David C.; Trend, Raissa M.; Genet, Cedric; McGrath, Matthew J.; O'Brien, Peter; Stoltz, Brian M.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 34 p. 6367 - 6370
反应条件
(R)-5-CF3-2-Ph-2,3-dihydroimidazo[1,2-a]pyridine; N-ethyl-N,N-diisopropylamine in chloroform 8 h; cooling; Title compound not separated from byproducts;
参考文献
Birman, Vladimir B.; Li, Ximin
Organic Letters, 2006 , vol. 8, # 7 p. 1351 - 1354
反应条件
triethylamine; planar-chiral DMAP derivative in 1,1-dimethylpropan-1-ol T=0°C; Acetylation; 25.5 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 9 p. 2794 - 2795
反应条件
chiral 2-(3',5'-di-t-butylPh)-2-phosphabicyclo[3.3.0]octane in n-heptane T=-40°C; 14 h; Title compound not separated from byproducts;
参考文献
Vedejs, Edwin; Daugulis, Olafs
Journal of the American Chemical Society, 2003 , vol. 125, # 14 p. 4166 - 4173
反应条件
N-ethyl-N,N-diisopropylamine; CF3-PIP in chloroform T=0°C; 8.25 h; Resolution of racemate; Product distribution / selectivity;
参考文献
Li, Ximin; Jiang, Hui; Uffman, Eric W.; Guo, Lei; Zhang, Yuhua; Yang, Xing; Birman, Vladimir B.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 1722 - 1737
反应条件
(R)-(+)-N-methylbenzoguanidine; trimethylacetic anhydride in diethyl ether T=20°C; 12 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Nakata, Kenya; Shiina, Isamu
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7092 - 7096
反应条件
Escherichia coli BioH in hexane T=35°C; 28 h; Resolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Wang, Bo; Tang, Xiaoling; Liu, Ji; Yu, Hongwei
Tetrahedron Letters, 2010 , vol. 51, # 48 p. 6360 - 6364
