1-(2-甲基苯基)乙醇合成路线 (共 64 条)
反应条件
ChiroCLEC-PC in toluene 239.25 h;
参考文献
Vedejs; Rozners
Journal of the American Chemical Society, 2001 , vol. 123, # 10 p. 2428 - 2429
反应条件
chiral substituted phosphabicyclo[3.3.0]octane*HBF4; triethylamine in 1,1-dimethylpropan-1-ol; dichloromethane T=-25°C; 20.2 h; Title compound not separated from byproducts;
参考文献
Duffey, Trisha A.; MacKay, James A.; Vedejs, Edwin
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4674 - 4685
反应条件
in water 24 h; Geotrichum candidum IFO 5767, without and with allyl alcohol as an additive; Product distribution;
参考文献
Nakamura, Kaoru; Fujii, Mikio; Ida, Yoshiteru
Tetrahedron Asymmetry, 2001 , vol. 12, # 22 p. 3147 - 3153
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene T=40°C; 15 h;
参考文献
Ghanem, Ashraf; Schurig, Volker
Monatshefte fur Chemie, 2003 , vol. 134, # 8 p. 1151 - 1157
反应条件
Pseudomonas cepacia lipase; 4 A molecular sieve; peracetylated-β-cyclodextrin in toluene T=40°C; 8 h; Title compound not separated from byproducts;
参考文献
Ghanem, Ashraf; Schurig, Volker
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2547 - 2555
参考文献
Nakamura, Kaoru; Inoue, Yuko; Matsuda, Tomoko; Misawa, Ibuki
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 16 p. 2397 - 2402
反应条件
aluminium trichloride in hexane; toluene T=-5°C; 17 h; Title compound not separated from byproducts;
参考文献
Kashima, Choji; Mizuhara, Saori; Miwa, Yohei; Yokoyama, Yukihiro
Tetrahedron Asymmetry, 2002 , vol. 13, # 16 p. 1713 - 1719
反应条件
Pseudomonas cepacia lipase; 4 A molecular sieve; peracetylated-β-cyclodextrin in toluene T=40°C; 2 h; Title compound not separated from byproducts;
参考文献
Ghanem, Ashraf; Schurig, Volker
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2547 - 2555
反应条件
1: With chiral 4-diethylaminopyridine-based reagent; triethylamine T=-78°C; 6.6 h; 2: in methanol T=-78 - 20°C; 0.25 h; Title compound not separated from byproducts;
参考文献
Spivey, Alan C.; Arseniyadis, Stellios; Fekner, Tomasz; Maddaford, Adrian; Leese, David P.
Tetrahedron, 2006 , vol. 62, # 2-3 p. 295 - 301
反应条件
4 A molecular sieve; chiral diamine; triethylamine in dichloromethane T=-78°C; 3 h; Yield givenYields of byproduct given;
参考文献
Sano, Tomohumi; Imai, Keisuke; Ohashi, Kousaburo; Oriyama, Takeshi
Chemistry Letters, 1999 , # 3 p. 265 - 266