反应条件
1: 100 percent / Et3N / CH2Cl2 / 0.17 h / -5 - 0 °C
2: 74 percent / LiN3, P(NMe2)3 / dimethylsulfoxide / Ambient temperature
3: H2 / Lindlar's catalyst / butan-1-ol / 3 h / 760 Torr
4: Et3N / butan-1-ol / 20 h / Heating
5: conc. HCl / 42 h / Ambient temperature
6: 70 percent / liquid NH3 / methanol / 18 h / 60 °C
7: 50 percent / 1 M BCl3 / CH2Cl2; hexane / 2.5 h / -75 °C
View Scheme
参考文献
Marquez, Victor E.; Lim, Mu-Ill; Tseng, Christopher K.-H.; Markovac, Anica; Priest, Matthew A.; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 24 p. 5709 - 5714
