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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
瓶型酵母A
合成路线
（共 98 条）
160343-79-3
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 2: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
160343-78-2
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 100 percent / DIBAL / toluene / -78 °C 2: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 3: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-52-2
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 97 percent / imidazole / dimethylformamide 2: 80 percent / OsO4, NMO / H2O; tetrahydrofuran 3: 100 percent / PPTS / acetone 4: 95 percent / Zn, AcOH / methanol 5: 97 percent / diphenyl ether / 0.5 h / Heating 6: 83 percent / PDC / CH2Cl2 7: 100 percent / DIBAL / toluene / -78 °C 8: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 9: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-48-6
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 100 percent / K2CO3 / methanol 2: 100 percent / N-bromosuccinimide / CH2Cl2 3: 97 percent / imidazole / dimethylformamide 4: 80 percent / OsO4, NMO / H2O; tetrahydrofuran 5: 100 percent / PPTS / acetone 6: 95 percent / Zn, AcOH / methanol 7: 97 percent / diphenyl ether / 0.5 h / Heating 8: 83 percent / PDC / CH2Cl2 9: 100 percent / DIBAL / toluene / -78 °C 10: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 11: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-59-9
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 100 percent / PPTS / acetone 2: 95 percent / Zn, AcOH / methanol 3: 97 percent / diphenyl ether / 0.5 h / Heating 4: 83 percent / PDC / CH2Cl2 5: 100 percent / DIBAL / toluene / -78 °C 6: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 7: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-56-6
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 80 percent / OsO4, NMO / H2O; tetrahydrofuran 2: 100 percent / PPTS / acetone 3: 95 percent / Zn, AcOH / methanol 4: 97 percent / diphenyl ether / 0.5 h / Heating 5: 83 percent / PDC / CH2Cl2 6: 100 percent / DIBAL / toluene / -78 °C 7: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 8: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-62-4
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 95 percent / Zn, AcOH / methanol 2: 97 percent / diphenyl ether / 0.5 h / Heating 3: 83 percent / PDC / CH2Cl2 4: 100 percent / DIBAL / toluene / -78 °C 5: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 6: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-64-6
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 97 percent / diphenyl ether / 0.5 h / Heating 2: 83 percent / PDC / CH2Cl2 3: 100 percent / DIBAL / toluene / -78 °C 4: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 5: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-80-6
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 100 percent / N-bromosuccinimide / CH2Cl2 2: 97 percent / imidazole / dimethylformamide 3: 80 percent / OsO4, NMO / H2O; tetrahydrofuran 4: 100 percent / PPTS / acetone 5: 95 percent / Zn, AcOH / methanol 6: 97 percent / diphenyl ether / 0.5 h / Heating 7: 83 percent / PDC / CH2Cl2 8: 100 percent / DIBAL / toluene / -78 °C 9: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 10: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
210897-66-8
→
反应条件
72877-50-0
瓶型酵母A
反应条件
1: 83 percent / PDC / CH2Cl2 2: 100 percent / DIBAL / toluene / -78 °C 3: 84 percent / diisopropyl azodicarboxylate, PPh3 / tetrahydrofuran 4: 90 percent / aq. HCl / methanol / 3 h / Ambient temperature View Scheme
参考文献
Yoshida, Naoyuki; Kamikubo, Takashi; Ogasawara, Kunio
Tetrahedron Letters, 1998 , vol. 39, # 26 p. 4677 - 4678
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