O,O′-二(三甲基甲硅烷基)胸苷合成路线 （共 89 条）
反应条件
in 1,2-dichloro-ethane T=30 - 50°C;
参考文献
Zhuk, R. A.; Ludzisha, A. S.; Kostyanovskii, R. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 1 p. 74 - 77
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 1 p. 90 - 93
反应条件
1: 55 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.5 h / Ambient temperature 2: 80 percent / conc. aq. NH4OH / methanol / 24 h View Scheme
参考文献
Lewis; Revankar; Hogan
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 5 p. 1309 - 1316
反应条件
1: 93 percent / SnCl4 / acetonitrile 2: 94 percent / K2CO3, MeOH / Heating 3: 81 percent / pyridine 4: 66 percent / iPr2NEt / tetrahydrofuran View Scheme
参考文献
Rizzo; Dougherty; Breslow
Tetrahedron Letters, 1992 , vol. 33, # 29 p. 4129 - 4132
反应条件
tin(IV) chloride in acetonitrile
参考文献
Rizzo; Dougherty; Breslow
Tetrahedron Letters, 1992 , vol. 33, # 29 p. 4129 - 4132
反应条件
1: 94 percent / SnCl4 / acetonitrile / 20 °C 2: 33 percent / 3,6-dimethyl-9-methylcarbazole; Mg(ClO4)2 / propan-2-ol; H2O / Photolysis View Scheme
参考文献
Wang, Zhiwei; Prudhomme, Daniel R.; Buck, Jason R.; Park, Minnie; Rizzo, Carmelo J.
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 5969 - 5985
参考文献
De Wall, Stephen L.; Barbour, Leonard J.; Schall, Otto F.; Gokel, George W.
Journal of Chemical Crystallography, 2000 , vol. 30, # 4 p. 227 - 231
参考文献
Fenick, David J.; Falvey, Daniel E.
Journal of Organic Chemistry, 1994 , vol. 59, # 17 p. 4791 - 4799
反应条件
water T=20°C; Alkylation; desilylation; 9 h;
参考文献
Edward Lindsell; Murray, Christopher; Preston, Peter N.; Woodman, Thomas A. J.
Tetrahedron, 2000 , vol. 56, # 9 p. 1233 - 1245
反应条件
1: SnCl4 / 1,2-dichloro-ethane / 1.) 0 deg C, 20 min, 2.) room temp., 20 h 2: O2, Rose Bengal / methanol / 0 °C / Irradiation View Scheme
参考文献
Feringa, Ben L.; Dannenberg, W.
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 6 p. 192 - 196
反应条件
1: 96 percent / p-nitrophenol / CHCl3 / 12 h / 30 °C 2: ammonia / methanol / 16 h / 30 °C View Scheme
参考文献
Aoyama
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2073 - 2077
