2-(4-硝基苯基)-1H-苯并咪唑合成路线 （共 52 条）
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
Heating;
参考文献
Tandon, Vishnu K.; Kumar, Manoj
Tetrahedron Letters, 2004 , vol. 45, # 21 p. 4185 - 4187
反应条件
[2,2']bipyridinyl; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; copper(l) chloride in neat (no solvent)
T=20°C; 11 h; Green chemistry;
参考文献
Yu, Jiatao; Xu, Jian; Lu, Ming
Applied Organometallic Chemistry, 2013 , vol. 27, # 10 p. 606 - 610
反应条件
1,3,2-benzodithiazole 1,1,3,3-tetraoxide in neat (no solvent)
T=20 - 25°C; 5 h; Green chemistry;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Arkivoc, 2012 , vol. 2012, # 9 p. 262 - 279
反应条件
N-ethyl-N,N-diisopropylamine; p-toluenesulfonyl chloride in dichloromethane
T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Lin, Chia-Chi; Hsieh, Tsung-Han; Liao, Pen-Yuan; Liao, Zhen-Yuan; Chang, Chih-Wei; Shih, Yu-Chiao; Yeh, Wen-Hsiung; Chien, Tun-Cheng
Organic Letters, 2014 , vol. 16, # 3 p. 892 - 895
反应条件
in 2,2,2-trifluoroethanol
T=80°C; 0.5 h;
参考文献
Chebolu, Rajesh; Kommi, Damodara N.; Kumar, Dinesh; Bollineni, Narendra; Chakraborti, Asit K.
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10158 - 10167
参考文献
Ramana, Devalla V.; Kantharaj, Ethirajulu
Tetrahedron, 1994 , vol. 50, # 8 p. 2485 - 2496
反应条件
sodium hydrogencarbonate; copper(I) bromide in dimethyl sulfoxide
T=120°C; 24 h;
参考文献
Qiu, Dezhi; Wei, Haidong; Zhou, Lihong; Zeng, Qingle
Applied Organometallic Chemistry, 2014 , vol. 28, # 2 p. 109 - 112
反应条件
sodium azide; N,N,N',N,-tetramethylethylenediamine; copper(l) chloride in dimethyl sulfoxide
T=120°C; 12 h;
参考文献
Kim, Yong; Kumar, Manian Rajesh; Park, Namjin; Heo, Yumi; Lee, Sunwoo
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9577 - 9583
反应条件
1: With copper(l) iodide; K3PO4*3H2O; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane
T=100°C; 3 h; Schlenk techniqueSealed tubeInert atmosphere;
2: With acetic acid in 1,4-dioxane
Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Yuan, Hua; Chen, Yongxin; Song, Jinli; Chen, Chunxia; Chen, Baohua
Chinese Journal of Chemistry, 2013 , vol. 31, # 10 p. 1247 - 1249
反应条件
1: alcohol
2: glacial acetic acid
View Scheme
参考文献
Hinsberg; Funcke
Chemische Berichte, 1894 , vol. 27, p. 2188
