4’-甲氧基[1,1’-联苯]-4-甲酸甲酯合成路线 (共 70 条)
反应条件
potassium phosphate; Ni(PCy3)2Cl2; water; tri-cyclo-hexyl-phosphine in 1,4-dioxane T=110°C; 12 h; Inert atmosphere;
参考文献
Guan, Bing-Tao; Wang, Yang; Li, Bi-Jie; Yu, Da-Gang; Shi, Zhang-Jie
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14468 - 14470
反应条件
manganese; cobalt (II) bromide; triphenylphosphine; trifluoroacetic acid in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 11 p. 2089 - 2092
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=110°C; Inert atmosphere;
参考文献
Wilson, Daniela A.; Wilson, Christopher J.; Rosen, Brad M.; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 21 p. 4879 - 4882
反应条件
potassium fluoride; palladium diacetate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=120°C;
参考文献
Hatanaka, Yasuo; Goda, Ken-ichi; Okahara, Yoshinori; Hiyama, Tamejiro
Tetrahedron, 1994 , vol. 50, # 28 p. 8301 - 8316
反应条件
1: (p-methoxyphenyl)(phenyl)iodonium tetrafluoroborate; polymer bound phenylboronate With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=20°C; Substitution; 20 h; 2: sodium methylate in tetrahydrofuran; methanol transesterification; 20 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 19 p. 3645 - 3655
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 16 h;
参考文献
Kasuga, Jun-Ichi; Ishikawa, Minoru; Yonehara, Mitsuhiro; Makishima, Makoto; Hashimoto, Yuichi; Miyachi, Hiroyuki
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 20 p. 7164 - 7173
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
反应条件
1: 4-iodo-benzoic acid methyl ester With lithium chloride in N,N-dimethyl-formamide T=80°C; 2: para-iodoanisole With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in N,N-dimethyl-formamide T=80°C; 2 h; Inert atmosphere;
参考文献
Papoian, Vardan; Minehan, Thomas
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7376 - 7379
反应条件
bis-triphenylphosphine-palladium(II) chloride; cesium fluoride in N,N-dimethyl-formamide T=80°C; Suzuki-Miyaura cross-coupling; 2 h; Inert atmosphere;
参考文献
PraveenGanesh, Nageswaran; Chavant, Pierre Yves
European Journal of Organic Chemistry, 2008 , # 27 p. 4690 - 4696
反应条件
palladium diacetate; cesium fluoride in water T=80°C; Suzuki reaction; 22 h;
参考文献
Miao, Weishi; Chan, Tak Hang
Organic Letters, 2003 , vol. 5, # 26 p. 5003 - 5005