4-甲氧基-N,N-二甲基-苯甲酰胺合成路线 (共 45 条)
反应条件
sodium hydroxide; trichlorophosphate
参考文献
Ienaga; Kazuharu; Nakamura; Ko
Patent: US4708961 A1, 1987 ;
反应条件
1: With disodium hydrogenphosphate in acetonitrile T=20°C; Methylation; 2: With disodium hydrogenphosphate Hydrolysis; 18 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
dibenzoyl peroxide in tetrachloromethane Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 24, # 26 p. 2685 - 2688
反应条件
tert.-butylhydroperoxide; 5,10,15,20-tetrakisphenylporphyrinatoiron(III) chloride in dichloromethane T=30°C; Kinetics;
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane T=-78°C; 1.5 h; Inert atmosphere; 2: With ammonia; iodine in tetrahydrofuran; hexane; water T=0 - 20°C; Inert atmosphere;
参考文献
Suzuki, Yusuke; Yoshino, Takumi; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2011 , vol. 67, # 21 p. 3809 - 3814
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water
T=90°C; 12 h;
参考文献
Li, Huamin; Xie, Jin; Xue, Qicai; Cheng, Yixiang; Zhu, Chengjian
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6479 - 6482,4
反应条件
oxygen; sodium hydroxide in water
T=25°C; 24 h;
参考文献
Wang, Wentao; Cong, Yu; Zhang, Leilei; Huang, Yanqiang; Wang, Xiaodong; Zhang, Tao
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 124 - 127
反应条件
sodium iodide in dimethyl sulfoxide
T=20°C; Electrochemical reaction;
参考文献
Huang, Haolai; Yuan, Gaoqing; Li, Xianwei; Jiang, Huanfeng
Tetrahedron Letters, 2013 , vol. 54, # 52 p. 7156 - 7159
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane
T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
反应条件
sodium methylate; nickel diacetate in 1,4-dioxane
T=110°C;
参考文献
Ju, Jinhun; Jeong, Miso; Moon, Jeongju; Hyun, Min Jung; Lee, Sunwoo
Organic Letters, 2007 , vol. 9, # 22 p. 4615 - 4618