4-甲氧基-N,N-二甲基-苯甲酰胺合成路线 （共 45 条）
反应条件
hydrogenchloride; tert.-butylhydroperoxide; iodine in cyclohexane; water
T=70 - 80°C; 20 h;
参考文献
Gao, Lingfeng; Tang, Haoming; Wang, Zhiyong
Chemical Communications, 2014 , vol. 50, # 31 p. 4085 - 4088
反应条件
1,4-diaza-bicyclo[2.2.2]octane; tert.-butylhydroperoxide; copper dichloride in water; 1,2-dichloro-ethane
T=80°C; Schlenk techniqueInert atmosphere; MechanismCatalytic behavior; Reagent/catalystTemperature;
参考文献
Xie, Ye-Xiang; Song, Ren-Jie; Yang, Xu-Heng; Xiang, Jian-Nan; Li, Jin-Heng
European Journal of Organic Chemistry, 2013 , # 25 p. 5737 - 5742
反应条件
T=160 - 210°C; P=1 Torr;
参考文献
Schroth, Werner; Krieg, Reimar; Kluge, Helmut; Gaebler, Michael
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 11 p. 398 - 399
反应条件
1: trifluoro acetic acid methyl ester With cesium fluoride; copper(l) iodide in N,N-dimethyl-formamide
T=130°C; 2 h;
2: para-iodoanisole; N,N-dimethyl-formamide T=180°C; 4 h; Further stages.;
参考文献
Langlois, Bernard R.; Roques, Nicolas
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1318 - 1325
反应条件
copper(I) oxide; 1,10-phenanthroline; oxygen; toluene-4-sulfonic acid
T=140°C; P=760.051 Torr; 24 h; Sealed tube;
参考文献
Hu, Chenxu; Yan, Xufei; Zhou, Xiangge; Li, Zhengkai
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 47 p. 8179 - 8182
反应条件
in toluene
T=100°C; 8 h;
参考文献
Cunico, Robert F.; Maity, Bikash C.
Organic Letters, 2002 , vol. 4, # 24 p. 4357 - 4359
反应条件
1: 7 percent Chromat. / cesium fluoride / copper(I) iodide / dimethylformamide / 8 h / 180 °C
2: 37 percent Chromat. / cesium fluoride / copper(I) iodide / 4 h / 180 °C
View Scheme
参考文献
Langlois, Bernard R.; Roques, Nicolas
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1318 - 1325
反应条件
1: palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; sodium acetate; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4; N,N-dicyclohexylmethylamine / ethylene glycol dimethyl ether / 18 h / 85 °C
2: pyridine; triethylamine / 26 h / 70 °C
View Scheme
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
反应条件
cesium fluoride; copper(l) iodide
T=180°C; 4 h;
参考文献
Langlois, Bernard R.; Roques, Nicolas
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1318 - 1325
反应条件
cesium fluoride; copper(I) bromide
T=180°C; 4 h;
参考文献
Langlois, Bernard R.; Roques, Nicolas
Journal of Fluorine Chemistry, 2007 , vol. 128, # 10 p. 1318 - 1325
